4,4-Dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole

Base Information

Chemical Name:4,4-Dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole
CAS No.:70165-35-4
Molecular Formula:C17H18N2
Molecular Weight:250.343
Hs Code.:
DSSTox Substance ID:DTXSID50602871
Wikidata:Q82500069

Synonyms:70165-35-4;4,4-Dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole;SCHEMBL3315653;DTXSID50602871

Suppliers and Price of 4,4-Dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4,4-Dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:250.146998583
Heavy Atom Count:19
Complexity:333

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1(CN(C(=N1)C2=CC=CC=C2)C3=CC=CC=C3)C

Technology Process of 4,4-Dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole

There total 6 articles about 4,4-Dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: N'-acetoxy-N-isobutyl-N-phenylbenzimidamide

: 70165-35-4
4,4-dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole

Guidance literature:: With potassium phosphate; copper(l) iodide; In toluene; at 100 ℃; for 5h; under 760.051 Torr; Inert atmosphere;
DOI:10.1039/c3ob41871e

Reference yield: 19.0%

: 1416437-39-2
N-isobutyl-N-phenylbenzimidamide

: 70165-35-4
4,4-dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole

Guidance literature:: With potassium phosphate; 1,10-Phenanthroline; [bis(acetoxy)iodo]benzene; copper diacetate; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol303302r

Reference yield:

: 588-47-6
N-isobutylaniline

: 100-47-0
benzonitrile

: 70165-35-4
4,4-dimethyl-1,2-diphenyl-4,5-dihydro-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethylaluminum / toluene / 1 h / 0 - 20 °C

1.2: 20 h / 100 °C

2.1: copper diacetate; potassium phosphate; [bis(acetoxy)iodo]benzene; 1,10-Phenanthroline / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With potassium phosphate; 1,10-Phenanthroline; [bis(acetoxy)iodo]benzene; trimethylaluminum; copper diacetate; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol303302r