2-Iodo-5-(trifluoromethyl)benzyl alcohol

Base Information

• Chemical Name: 2-Iodo-5-(trifluoromethyl)benzyl alcohol
• CAS No.: 702641-05-2
• Molecular Formula: C8H6F3IO
• Molecular Weight: 302.035
• Hs Code.: 2906290090
• Mol file: 702641-05-2.mol

Synonyms:BENZENEMETHANOL,2-IODO-5-(TRIFLUOROMETHYL);2-iodo-5-(trifluoromethyl)phenylmethanol;5-trifluoromethyl-2-iodobenzyl alcohol;2-Iodo-5-trifluoromethylbenzyl alcohol;

Chemical Property of 2-Iodo-5-(trifluoromethyl)benzyl alcohol

Chemical Property:

• Melting Point: 81-82℃
• Boiling Point: 271℃
• PKA: 13.82±0.10(Predicted)
• Flash Point: 118℃
• PSA: 20.23000
• Density: 1.901
• LogP: 2.80230
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99%, ^*data from raw suppliers

2-Iodo-5-(trifluoromethyl)benzylAlcohol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Iodo-5-(trifluoromethyl)benzyl alcohol

There total 8 articles about 2-Iodo-5-(trifluoromethyl)benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-iodo-5-(trifluoromethyl)benzoic acid (702641-04-1) → [2-iodo-5-(trifluoromethyl)phenyl]methanol (702641-05-2)

Guidance literature:

With sodium tetrahydroborate; iodine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/acs.joc.0c01125

Reference yield:

2-iodo-5-(trifluoromethyl)benzaldehyde (875446-23-4) → [2-iodo-5-(trifluoromethyl)phenyl]methanol (702641-05-2)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; water; at 0 ℃; for 0.5h;

Reference yield:

2-Amino-5-(trifluoromethyl)benzyl alcohol (220107-65-3) → [2-iodo-5-(trifluoromethyl)phenyl]methanol (702641-05-2)

Guidance literature:

2-Amino-5-(trifluoromethyl)benzyl alcohol; With sulfuric acid; acetic acid; sodium nitrite; for 0.5h;

With potassium iodide; In water; at 70 ℃; for 0.5h;

upstream raw materials:

2-iodo-5-(trifluoromethyl)benzoic acid

2-iodo-5-(trifluoromethyl)benzaldehyde

2-Amino-5-(trifluoromethyl)benzyl alcohol

2-iodo-5-(trifluoromethyl)benzonitrile

Downstream raw materials:

2-(bromomethyl)-1-iodo-4-(trifluoromethyl)benzene

(+)-(5R)-5-[3,5-bis(trifluoromethyl)phenyl]-3-{[4'-fluoro-2'-methoxy-5'-(propan-2-yl)-4-(trifluoromethyl)biphenyl-2-yl]methyl}-4,4-dimethyl-1,3-oxazolidin-2-one

(-)-(5S)-5-[3,5-bis(trifluoromethyl)phenyl]-3-{[4'-fluoro-2'-methoxy-5'-(propan-2-yl)-4-(trifluoromethyl)biphenyl-2-yl]methyl}-4,4-dimethyl-1,3-oxazolidin-2-one

(+)-(4S,5R)-5-[3,5-bis(trifluoromethyl)phenyl]-3-{[4'-fluoro-2'-methoxy-5'-(propan-2-yl)-4-(trifluoromethyl)biphenyl-2-yl]methyl}-4,5-dimethyl-1,3-oxazolidin-2-one

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