21-ethyl-4-methylatid-16-en-15-ol

Base Information

• Chemical Name: 21-ethyl-4-methylatid-16-en-15-ol
• CAS No.: 1634-83-9
• Molecular Formula: C₂₂H₃₅NO
• Molecular Weight: 329.526
• Mol file: 1634-83-9.mol

Synonyms:Atidine,21-de(2-hydroxyethyl)-7-deoxo-21-ethyl- (8CI); Atisine,N-de(2-hydroxyethyl)-N-ethyldihydro- (7CI);1H,7H-6a,9-Ethano-4,10b-propanobenz[h]isoquinoline, atidan-15-ol deriv.; NSC406048

Chemical Property of 21-ethyl-4-methylatid-16-en-15-ol

Chemical Property:

• Vapor Pressure: 6.83E-10mmHg at 25°C
• Boiling Point: 447.6°Cat760mmHg
• Flash Point: 49.7°C
• Density: 1.1g/cm³

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 21-ethyl-4-methylatid-16-en-15-ol

There total 5 articles about 21-ethyl-4-methylatid-16-en-15-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N-Ethyl-N-des-(β-hydroxy-ethyl)-dihydro-15-epiatisin (1634-83-9)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

DOI:10.1021/ja01082a017

Reference yield:

N-Acetyl 15-acetoxy-16,17-didehydro-4-methylatidane (910-09-8) → N-Ethyl-N-des-(β-hydroxy-ethyl)-dihydro-atisin (1634-83-9)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

DOI:10.1021/ja01082a017

Reference yield:

ethyl iodide (75-03-6) → N-Ethyl-N-des-(β-hydroxy-ethyl)-dihydro-atisin (1634-83-9)

Guidance literature:

With methanol; sodium carbonate;

DOI:10.1021/ja01082a017

upstream raw materials:

N-Acetyl 15-acetoxy-16,17-didehydro-4-methylatidane

ethyl iodide

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