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High purity Iodoethane CAS 75-03-6 with competitive price
Cas No: 75-03-6
USD $ 60.0-60.0 / Kilogram 25 Kilogram 10000 Metric Ton/Month Wuhan Fortuna Chemical Co.,Ltd Contact Supplier
Iodoethane
Cas No: 75-03-6
No Data 100 Kilogram 100 Metric Ton/Month Suzhou Sinosun Imp.&Exp. Corporation Contact Supplier
Factory Supply Iodoethane
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No Data 1 1 Ality Chemical Corporation Contact Supplier
Amadis Chemical offer CAS#75-03-6;CAT#A838307
Cas No: 75-03-6
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
High purity Iodoethane 98% TOP1 supplier in China
Cas No: 75-03-6
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
Iodoethane CAS: 75-03-6
Cas No: 75-03-6
USD $ 1.0-2.0 / Metric Ton 5 Metric Ton 1000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
Iodoethane 75-03-6
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Iodoethane
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USD $ 12.0-12.0 / Metric Ton 1 Metric Ton 50 Metric Ton/Year Jinan Finer Chemical Co., Ltd Contact Supplier
Iodoethane
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Iodoethane Hydrocarbons halides
Cas No: 75-03-6
USD $ 35.0-50.0 / Kilogram 1 Kilogram 10000 Metric Ton/Month Baoji Guokang Healthchem co.,ltd Contact Supplier

75-03-6 Usage

InChI:InChI=1/C2H5I/c1-2-3/h2H2,1H3

75-03-6 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (I0058)  Iodoethane (stabilized with Copper chip)  >99.0%(GC) 75-03-6 25g 170.00CNY Detail
TCI America (I0058)  Iodoethane (stabilized with Copper chip)  >99.0%(GC) 75-03-6 100g 410.00CNY Detail
TCI America (I0058)  Iodoethane (stabilized with Copper chip)  >99.0%(GC) 75-03-6 500g 990.00CNY Detail
Alfa Aesar (A14444)  Iodoethane, 98+%, stab. with copper    75-03-6 100g 281.0CNY Detail
Alfa Aesar (A14444)  Iodoethane, 98+%, stab. with copper    75-03-6 500g 1110.0CNY Detail
Alfa Aesar (A14444)  Iodoethane, 98+%, stab. with copper    75-03-6 2500g 4434.0CNY Detail

75-03-6SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name iodoethane

1.2 Other means of identification

Product number -
Other names Ethane,iodo

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:75-03-6 SDS

75-03-6Synthetic route

[CoEt(dimethylglyoximate(1-))2(pyridine)]

[CoEt(dimethylglyoximate(1-))2(pyridine)]

iodine
7553-56-2

iodine

A

iodobisdimethylglyoximepyridine cobalt(III)

iodobisdimethylglyoximepyridine cobalt(III)

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
In tetrachloromethane Kinetics; Irradiation (UV/VIS); Kinetics of the reaction of Co(C2H5)(H3CCNOHONCCH3)2(C5H5N) with I2 under irradiation with light at 517 nm is investigated.; MeI and CoI(H3CCNOHONCCH3)2(C5H5N) are the products.;A n/a
B 100%
[CoEt(dimethylglyoximate(1-))2(pyridine)]

[CoEt(dimethylglyoximate(1-))2(pyridine)]

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
With iodine In acetonitrile Kinetics; byproducts: {Co(bis(dimethylglyoximato))py(I)}; one-electron oxidn. of Co complex by I2 at 298 K; monitored by (1)H-NMR and UV spect. (361 nm);100%
ethyl 4-(diethoxyphosphorylmethyl)-5-(iodomethyl)furan-3-carboxylate

ethyl 4-(diethoxyphosphorylmethyl)-5-(iodomethyl)furan-3-carboxylate

triethyl phosphite
122-52-1

triethyl phosphite

A

ethylphosphonic acid diethyl ester
78-38-6

ethylphosphonic acid diethyl ester

B

ethyl 4,5-bis-(diethoxyphosphorylmethyl)furan-3-carboxylate

ethyl 4,5-bis-(diethoxyphosphorylmethyl)furan-3-carboxylate

C

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
at 90 - 170℃; for 0.166667h; Arbuzov Reaction;A n/a
B 98%
C n/a
triethyl phosphite
122-52-1

triethyl phosphite

methyl iodide
74-88-4

methyl iodide

A

Diethyl methylphosphonate
683-08-9

Diethyl methylphosphonate

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
at 130℃; for 0.0833333h; Michaelis-Arbuzov reaction; microwave irradiation;A 97%
B n/a
cis-{(C2H5)2Co(2,2'-bipyridine)2}(ClO4)

cis-{(C2H5)2Co(2,2'-bipyridine)2}(ClO4)

A

ethane
74-84-0

ethane

B

ethene
74-85-1

ethene

C

ethyl iodide
75-03-6

ethyl iodide

D

n-butane
106-97-8

n-butane

Conditions
ConditionsYield
With iodine In acetonitrile Kinetics; byproducts: I3(1-), {(C2H5)Co(2,2'-bipyridine)2I}(1+); one-electron oxidn. of cis-Co complex by I2 at 298 K; monitored by (1)H-NMR and UV spect. (361 nm);A <1
B <1
C 97%
D 3.2%
methoxyethene
107-25-5

methoxyethene

propargyl alcohol
107-19-7

propargyl alcohol

A

3-(1-methoxy-ethoxy)-propyne
38987-67-6

3-(1-methoxy-ethoxy)-propyne

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
With toluene-4-sulfonic acidA 96%
B n/a
iodobenzene
591-50-4

iodobenzene

triethyl phosphite
122-52-1

triethyl phosphite

A

diethyl phenylphosphonate
1754-49-0

diethyl phenylphosphonate

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
tetrakis(triethylphosphite)nickel(0) at 160℃;A 94%
B n/a
at 160℃; Mechanism; var. catalysts, var. temp.;
diethyl phosphoriodidite
20502-50-5

diethyl phosphoriodidite

N-(propylidene)-tert-butylamine
7020-81-7

N-(propylidene)-tert-butylamine

A

ethyl iodide
75-03-6

ethyl iodide

B

1,4-di-tert-butyl-2-ethoxy-3,5-diethyl-1,4,2-diazaphospholidine 2-oxide

1,4-di-tert-butyl-2-ethoxy-3,5-diethyl-1,4,2-diazaphospholidine 2-oxide

Conditions
ConditionsYield
In diethyl ether for 2h; Ambient temperature;A n/a
B 92%
trimethylsilyl iodide
16029-98-4

trimethylsilyl iodide

ethyl acetate
141-78-6

ethyl acetate

A

trimethylsilyl acetate
2754-27-0

trimethylsilyl acetate

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
at 100℃; for 0.5h; Mechanism; Product distribution;A n/a
B 92%
4-vinylbenzyl iodide
45817-37-6

4-vinylbenzyl iodide

triethyl phosphite
122-52-1

triethyl phosphite

A

[(4-ethenylphenyl)methyl]phosphonic acid diethyl ester
726-61-4

[(4-ethenylphenyl)methyl]phosphonic acid diethyl ester

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
at 20℃; for 6h;A 91%
B n/a
O,O-diethyl-N-butyl-N-isobutenyl aminophosphite
79948-06-4

O,O-diethyl-N-butyl-N-isobutenyl aminophosphite

A

ethyl iodide
75-03-6

ethyl iodide

B

ethyl N-butyl-N-isobutenylamidomethylphosphonate

ethyl N-butyl-N-isobutenylamidomethylphosphonate

Conditions
ConditionsYield
With methyl iodide at 20℃;A 90.5%
B 87.1%
O,O-diethyl-N-butyl-N-isobutenyl aminophosphite
79948-06-4

O,O-diethyl-N-butyl-N-isobutenyl aminophosphite

methyl iodide
74-88-4

methyl iodide

A

ethyl iodide
75-03-6

ethyl iodide

B

ethyl N-butyl-N-isobutenylamidomethylphosphonate

ethyl N-butyl-N-isobutenylamidomethylphosphonate

Conditions
ConditionsYield
at 20℃;A 90.5%
B 87.1%
diethyl phosphoriodidite
20502-50-5

diethyl phosphoriodidite

N-Benzylidenemethylamine
622-29-7

N-Benzylidenemethylamine

A

ethyl iodide
75-03-6

ethyl iodide

B

2-ethoxy-1,4-dimethyl-3,5-diphenyl-1,4,2-diazaphospholidine 2-oxide

2-ethoxy-1,4-dimethyl-3,5-diphenyl-1,4,2-diazaphospholidine 2-oxide

Conditions
ConditionsYield
In diethyl ether for 2h; Ambient temperature;A n/a
B 90%
cis-{(C2H5)2Co(2,2'-bipyridine)2}(ClO4)

cis-{(C2H5)2Co(2,2'-bipyridine)2}(ClO4)

iodine
7553-56-2

iodine

cis-ethyl iodo bis(2,2'-bipyridyl) cobalt(III) perchlorate

cis-ethyl iodo bis(2,2'-bipyridyl) cobalt(III) perchlorate

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
In tetrachloromethane Kinetics; byproducts: C4H10, C2H6; Irradiation (UV/VIS); Kinetics of the reaction of Co(C2H5)2(bipy)2ClO4 with I2 under irradiation with light at 517 nm is investigated.; EtI and Co(C2H5)I(bipy)2ClO4 are the main products, C4H10 and C2H6 are byproducts.;A n/a
B 90%
cis-{Et2Co(bpy)2}(1+)

cis-{Et2Co(bpy)2}(1+)

iodine
7553-56-2

iodine

A

ethane
74-84-0

ethane

B

ethyl iodide
75-03-6

ethyl iodide

C

n-butane
106-97-8

n-butane

Conditions
ConditionsYield
In tetrachloromethane Irradiation (UV/VIS); Irradiation at 509 nm in CCl4.; Estimation of the quantum yield of the photochemical reaction. Yield of the products estimated by g.l.c.;A <1
B 90%
C 10%
C26H39NO5Si

C26H39NO5Si

A

C28H43NO5Si

C28H43NO5Si

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
With lithium chloride; lithium hexamethyldisilazane In tetrahydrofuran at 0℃;A 88%
B n/a
3-ethyl-2-methylnaphtho[2,1-d]thiazol-3-ium iodide
54581-48-5

3-ethyl-2-methylnaphtho[2,1-d]thiazol-3-ium iodide

A

diethyl ether
60-29-7

diethyl ether

B

ethene
74-85-1

ethene

C

ethyl iodide
75-03-6

ethyl iodide

D

2-methyl-3-ethylnaphtho<2,1-d>thiazolium bisulfate

2-methyl-3-ethylnaphtho<2,1-d>thiazolium bisulfate

Conditions
ConditionsYield
With diethyl sulfate at 100℃; for 0.5h; Product distribution;A n/a
B n/a
C n/a
D 87%
With diethyl sulfate at 100℃; for 0.5h;A n/a
B n/a
C n/a
D 87%
trimethylsilyl iodide
16029-98-4

trimethylsilyl iodide

benzoic acid ethyl ester
93-89-0

benzoic acid ethyl ester

A

trimethylsilyl benzoate
2078-12-8

trimethylsilyl benzoate

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
at 100℃; for 0.5h; Mechanism; Product distribution;A n/a
B 86%
(5S,8R,9S,10S,13R,14S,17R)-3-Ethoxy-17-((1R,4R)-4-ethyl-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene
78371-07-0

(5S,8R,9S,10S,13R,14S,17R)-3-Ethoxy-17-((1R,4R)-4-ethyl-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthrene

A

ethyl iodide
75-03-6

ethyl iodide

B

sitostanol
204638-28-8

sitostanol

Conditions
ConditionsYield
With Methyltrichlorosilane; sodium iodide In acetonitrile at 25℃; for 36h;A n/a
B 86%
cyclohexyl ethyl ether
932-92-3

cyclohexyl ethyl ether

A

ethyl iodide
75-03-6

ethyl iodide

B

cyclohexanol
108-93-0

cyclohexanol

Conditions
ConditionsYield
With Methyltrichlorosilane; sodium iodide In acetonitrile at 25℃; for 8h;A n/a
B 85%
{(η5-C5H5)Re(NO)(PPh3)(IC2H5)}BF4

{(η5-C5H5)Re(NO)(PPh3)(IC2H5)}BF4

acetonitrile
75-05-8

acetonitrile

A

{(η5-C5H5)Re(NO)(PPh3)(NCCH3)}BF4

{(η5-C5H5)Re(NO)(PPh3)(NCCH3)}BF4

(RR,SS)-{(η5-C5H5)Re(NO)(PPh3)}2I(BF4)

(RR,SS)-{(η5-C5H5)Re(NO)(PPh3)}2I(BF4)

(SS,RR)-{(η5-C5H5)Re(NO)(PPh3)}2Cl(BF4)

(SS,RR)-{(η5-C5H5)Re(NO)(PPh3)}2Cl(BF4)

D

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
In dichloromethane-d2 (N2); Re complex in CD2Cl2 was reacted with CH3CN for 24 h; monitored by (1)H- and (31)P-NMR;A 85%
B n/a
C n/a
D 74%
trimethylsilyl iodide
16029-98-4

trimethylsilyl iodide

ethyl ester of p-toluenesulfonic acid
80-40-0

ethyl ester of p-toluenesulfonic acid

A

4-Methyl-1-benzolsulfonsaeure-trimethylsilylester
17872-98-9

4-Methyl-1-benzolsulfonsaeure-trimethylsilylester

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
at 100℃; for 0.5h; Mechanism; Product distribution;A n/a
B 84%
triethyl trithiophosphite
688-62-0

triethyl trithiophosphite

methyl iodide
74-88-4

methyl iodide

A

S,S-diethyl methylphosphonodithiothionate
31650-57-4

S,S-diethyl methylphosphonodithiothionate

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
at 20℃; for 3600h;A 64%
B 80%
for 288h; Ambient temperature;A 59%
B n/a
triethylamine
121-44-8

triethylamine

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
With 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; sodium iodide In acetone Reflux;80%
2-ethoxy-ethanol
110-80-5

2-ethoxy-ethanol

acetyl iodide
507-02-8

acetyl iodide

A

2-hydroxyethyl acetate
542-59-6

2-hydroxyethyl acetate

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
A 79%
B n/a
4-Ethoxy-octane
77067-57-3

4-Ethoxy-octane

A

octan-4-ol
589-62-8

octan-4-ol

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
With Methyltrichlorosilane; sodium iodide In acetonitrile at 25℃; for 8h;A 75%
B n/a
ethanol
64-17-5

ethanol

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
With hydrogen iodide at 120℃; for 2h;72%
With iodine; aluminium
With phosphorus; iodine
acetyl iodide
507-02-8

acetyl iodide

Phenetole
103-73-1

Phenetole

A

ethyl iodide
75-03-6

ethyl iodide

B

Phenyl acetate
122-79-2

Phenyl acetate

Conditions
ConditionsYield
at 20℃;A n/a
B 71%
1-methyl-1H-imidazole
616-47-7

1-methyl-1H-imidazole

ethyl iodide
75-03-6

ethyl iodide

1-ethyl-3-methylimidazolium iodide
35935-34-3

1-ethyl-3-methylimidazolium iodide

Conditions
ConditionsYield
In tetrahydrofuran for 4h; Heating;100%
In dichloromethane for 18h; Heating;98%
In tetrahydrofuran at 20℃; for 1h; Cooling with ice;97%
benzoimidazole
51-17-2

benzoimidazole

ethyl iodide
75-03-6

ethyl iodide

1,3-diethyl-1H-benzo[d]imidazol-3-ium iodide
24351-22-2

1,3-diethyl-1H-benzo[d]imidazol-3-ium iodide

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 70℃; for 24h;100%
With potassium carbonate In acetonitrile for 8h; Reflux;90%
With sodium acetate In o-xylene for 3h; Reflux;74%
1-methylquinoline-2(1H)-thione
4800-27-5

1-methylquinoline-2(1H)-thione

ethyl iodide
75-03-6

ethyl iodide

2-ethylthio-1-methylquinolinium iodide
95875-55-1

2-ethylthio-1-methylquinolinium iodide

Conditions
ConditionsYield
In benzene for 6h; Heating;100%
4-methoxy-aniline
104-94-9

4-methoxy-aniline

ethyl iodide
75-03-6

ethyl iodide

N,N-diethyl-4-methoxyaniline
15144-80-6

N,N-diethyl-4-methoxyaniline

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 15h;100%
With sodium hydroxide at 120℃;
ethyl iodide
75-03-6

ethyl iodide

Thiosalicylic acid
147-93-3

Thiosalicylic acid

2-ethylsulfanylbenzoic acid
21101-79-1

2-ethylsulfanylbenzoic acid

Conditions
ConditionsYield
With sodium hydroxide In ethanol at 20℃; for 15h;100%
With sodium hydroxide In ethanol at 20℃; for 15h;100%
With sodium hydroxide In ethanol; water for 72h;98%
ethyl iodide
75-03-6

ethyl iodide

Dimethyl(phenyl)phosphine
672-66-2

Dimethyl(phenyl)phosphine

dimethylethylphenylphosphonium iodide
72153-49-2

dimethylethylphenylphosphonium iodide

Conditions
ConditionsYield
In benzene at 20℃; for 12h; Inert atmosphere; Schlenk technique;100%
glyoxalic acid ethylthioacetal
10490-06-9

glyoxalic acid ethylthioacetal

ethyl iodide
75-03-6

ethyl iodide

2,2-bis(ethylthio)butanoic acid
71535-44-9

2,2-bis(ethylthio)butanoic acid

Conditions
ConditionsYield
With oxonium; potassium hexamethylsilazane In tetrahydrofuran at 25℃; for 2.5h; Product distribution; reactant;100%
(i) HN(SiMe3)2, KH, THF, (ii) /BRN= 505934/, (iii) aq. HCl; Multistep reaction;
With hydrogenchloride; potassium hydride; 1,1,1,3,3,3-hexamethyl-disilazane 1.) THF, 0 deg C, 15 min; THF, 25 deg C, 2.5 h.; Yield given. Multistep reaction;
mesitylenecarboxylic acid
480-63-7

mesitylenecarboxylic acid

ethyl iodide
75-03-6

ethyl iodide

ethyl 2,4,6-trimethylbenzoate
1754-55-8

ethyl 2,4,6-trimethylbenzoate

Conditions
ConditionsYield
With caesium carbonate In acetonitrile for 2h; Heating;100%
With cesium fluoride In acetonitrile for 1h; Heating;99%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In benzene
With potassium carbonate In acetone for 16h; Heating;
With cesium fluoride In N,N-dimethyl-formamide at 10 - 15℃; for 24h;88 % Chromat.
indole
120-72-9

indole

ethyl iodide
75-03-6

ethyl iodide

N-Ethylindole
10604-59-8

N-Ethylindole

Conditions
ConditionsYield
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Inert atmosphere;
Stage #2: ethyl iodide for 1h;
100%
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere;
Stage #2: ethyl iodide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere;
98%
Stage #1: indole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 0.5h;
Stage #2: ethyl iodide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃;
98%
2,3-dihydrobenzimidazol-2-thione
583-39-1

2,3-dihydrobenzimidazol-2-thione

ethyl iodide
75-03-6

ethyl iodide

1-ethyl-2-(ethylthio)-1H-benzo[d]imidazole
124530-66-1

1-ethyl-2-(ethylthio)-1H-benzo[d]imidazole

Conditions
ConditionsYield
With sodium naphthalenide In tetrahydrofuran for 5h; Ambient temperature;100%
1-(tert-butoxycarbonyl)-L-proline
15761-39-4

1-(tert-butoxycarbonyl)-L-proline

ethyl iodide
75-03-6

ethyl iodide

(2S)-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-ethyl ester
135097-23-3

(2S)-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-ethyl ester

Conditions
ConditionsYield
With potassium carbonate In acetone for 16h; Ambient temperature;100%
With 18-crown-6 ether; potassium carbonate In tetrahydrofuran for 21h; Inert atmosphere; Reflux;
indole-2,3-dione
91-56-5

indole-2,3-dione

ethyl iodide
75-03-6

ethyl iodide

N-ethylisatin
4290-94-2

N-ethylisatin

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 72h;100%
With potassium carbonate In N,N-dimethyl-formamide for 0.05h; microwave irradiation;90%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 12h; Inert atmosphere;90%
ortho-methylbenzoic acid
118-90-1

ortho-methylbenzoic acid

ethyl iodide
75-03-6

ethyl iodide

2-(n-Propyl)-benzoesaeure
2438-03-1

2-(n-Propyl)-benzoesaeure

Conditions
ConditionsYield
Stage #1: ortho-methylbenzoic acid With sec.-butyllithium In tetrahydrofuran; 1-hexene; cyclohexane at -78 - 20℃;
Stage #2: ethyl iodide In tetrahydrofuran; 1-hexene; cyclohexane at -78 - 20℃;
Stage #3: With hydrogenchloride; water In tetrahydrofuran; cyclohexane
100%
With sec.-butyllithium In cyclohexane for 8h; Ambient temperature;82%
With sec.-butyllithium 1.) THF, cyclohexane, -78 deg C, 1 h, 2.) THF, cyclohexane, RT, 4 h; Yield given. Multistep reaction;
BOC-glycine
4530-20-5

BOC-glycine

ethyl iodide
75-03-6

ethyl iodide

N-(tert-buytoxycarbonyl)-N-ethylglycine
149794-10-5

N-(tert-buytoxycarbonyl)-N-ethylglycine

Conditions
ConditionsYield
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0℃; for 1h;
Stage #2: In tetrahydrofuran at 0℃;
100%
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0 - 20℃;
Stage #2: With citric acid In water pH=2 - 3;
100%
Stage #1: BOC-glycine; ethyl iodide With sodium hydride In tetrahydrofuran at 0 - 20℃;
Stage #2: With citric acid In water pH=2 - 3;
100%
diphenyl sulfide
139-66-2

diphenyl sulfide

ethyl iodide
75-03-6

ethyl iodide

diphenylethylsulfonium perchlorate
10504-65-1

diphenylethylsulfonium perchlorate

Conditions
ConditionsYield
With silver perchlorate In acetonitrile for 48h; Ambient temperature;100%
methyl (2-nitrophenyl)acetate
30095-98-8

methyl (2-nitrophenyl)acetate

ethyl iodide
75-03-6

ethyl iodide

methyl 2-ethyl-2-(2-nitrophenyl)butanoate
136764-89-1

methyl 2-ethyl-2-(2-nitrophenyl)butanoate

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 4.5h;100%
With potassium tert-butylate; 18-crown-6 ether In tetrahydrofuran 1) -78 deg C to RT, 2 h, 2) -78 deg C;76%
diphenyl diselenide
1666-13-3

diphenyl diselenide

ethyl iodide
75-03-6

ethyl iodide

ethyl phenyl selenide
17774-38-8

ethyl phenyl selenide

Conditions
ConditionsYield
With dipotassium hydrogenphosphate; zinc In water; acetonitrile for 1h;100%
With dipotassium hydrogenphosphate; zinc In water; acetonitrile for 1h; Product distribution; Further Variations:; Reaction partners; Reagents; Solvents;100%
With sodium tetrahydroborate In acetonitrile for 0.0833333h; pH=7; pH-value;100%
5-hydroxy-5-(trifluoromethyl)imidazolidine-2,4-dione
105480-41-9

5-hydroxy-5-(trifluoromethyl)imidazolidine-2,4-dione

ethyl iodide
75-03-6

ethyl iodide

3-Ethyl-5-hydroxy-5-trifluoromethyl-imidazolidine-2,4-dione
105480-43-1

3-Ethyl-5-hydroxy-5-trifluoromethyl-imidazolidine-2,4-dione

Conditions
ConditionsYield
With sodium ethanolate In ethanol Ambient temperature;100%
With potassium carbonate In acetone Heating;60 % Turnov.
1-(tert-butoxycarbonylamino)-2,3-difluorobenzene
129589-65-7

1-(tert-butoxycarbonylamino)-2,3-difluorobenzene

ethyl iodide
75-03-6

ethyl iodide

N-(tert-Butoxycarbonyl)-N-ethyl-2,3-difluoroaniline
129589-69-1

N-(tert-Butoxycarbonyl)-N-ethyl-2,3-difluoroaniline

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide for 2h;100%
sel de potassium de la 2-phenyl-1,3,4-oxadiazol-5(4H)-one

sel de potassium de la 2-phenyl-1,3,4-oxadiazol-5(4H)-one

ethyl iodide
75-03-6

ethyl iodide

2-phenyl-4-ethyl-1,3,4-thiadiazol-5(4H)-one
82476-09-3

2-phenyl-4-ethyl-1,3,4-thiadiazol-5(4H)-one

Conditions
ConditionsYield
In acetonitrile for 5h; Heating;100%
imidazo[1,5-a]pyridine-3-thiol
76259-00-2

imidazo[1,5-a]pyridine-3-thiol

ethyl iodide
75-03-6

ethyl iodide

3-ethylsulfanyl-imidazo[1,5-a]pyridine
76266-04-1

3-ethylsulfanyl-imidazo[1,5-a]pyridine

Conditions
ConditionsYield
With potassium carbonate In acetone at 45℃;100%
With potassium carbonate In acetone at 45℃; for 12h;
With potassium carbonate In acetone Inert atmosphere;
1-benzyl-3-carbethoxy-5-methyl-7-phenyl-1,4-dihydro-4-oxopyrrolo<3,4-b>pyridine
100856-26-6

1-benzyl-3-carbethoxy-5-methyl-7-phenyl-1,4-dihydro-4-oxopyrrolo<3,4-b>pyridine

ethyl iodide
75-03-6

ethyl iodide

1-Benzyl-6-ethyl-5-methyl-4-oxo-7-phenyl-4,6-dihydro-1H-pyrrolo[3,4-b]pyridine-3-carboxylic acid ethyl ester
100856-34-6

1-Benzyl-6-ethyl-5-methyl-4-oxo-7-phenyl-4,6-dihydro-1H-pyrrolo[3,4-b]pyridine-3-carboxylic acid ethyl ester

Conditions
ConditionsYield
With sodium methylate In N,N-dimethyl-formamide r.t., overnight;100%
ethyl iodide
75-03-6

ethyl iodide

2-Mercaptobenzothiazole
149-30-4

2-Mercaptobenzothiazole

2-(ethylthio)benzothiazole
2757-92-8

2-(ethylthio)benzothiazole

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 6h;100%
With N-ethyl-N,N-diisopropylamine In acetone at 20℃; for 0.333333h; Sonication;90%
With potassium hydroxide In 1,4-dioxane at 70℃; for 1.5h;58%
ethyl iodide
75-03-6

ethyl iodide

2-methyl-3-trifluoroacetylpyrrole
142991-74-0

2-methyl-3-trifluoroacetylpyrrole

1-ethyl-3-trifluoroacetyl-2-methylpyrrole
144219-84-1

1-ethyl-3-trifluoroacetyl-2-methylpyrrole

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide at 40℃; for 20h;100%
ethyl iodide
75-03-6

ethyl iodide

(S)-2-hydroxy-4-pentenoic acid
38996-05-3

(S)-2-hydroxy-4-pentenoic acid

(S)-3-hydroxy-4-pentenoic acid ethyl ester
349649-09-8

(S)-3-hydroxy-4-pentenoic acid ethyl ester

Conditions
ConditionsYield
With sodium hydrogencarbonate In N,N-dimethyl-formamide for 5h;100%
ethyl iodide
75-03-6

ethyl iodide

3-trifluoroacetyl-2-phenylpyrrole
144219-80-7

3-trifluoroacetyl-2-phenylpyrrole

1-ethyl-3-trifluoroacetyl-2-phenylpyrrole
144219-86-3

1-ethyl-3-trifluoroacetyl-2-phenylpyrrole

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide at 70℃; for 20h;100%
ethyl iodide
75-03-6

ethyl iodide

2-amino-benzenethiol
137-07-5

2-amino-benzenethiol

2-(ethylthio)aniline
13920-91-7

2-(ethylthio)aniline

Conditions
ConditionsYield
With sodium hydride In acetonitrile at 0℃; for 7h;100%
With sodium methylate In methanol for 6h; Reflux;97%
Stage #1: 2-amino-benzenethiol With potassium tert-butylate In ethanol at 0℃; for 0.75h;
Stage #2: ethyl iodide In ethanol at 0 - 20℃; for 0.75h; Further stages.;
85%
ethyl iodide
75-03-6

ethyl iodide

C10H21N4PS2

C10H21N4PS2

1-Ethylsulfanylthiocarbonyl-2,8,9-trimethyl-2,5,8,9-tetraaza-1-phosphonia-bicyclo[3.3.3]undecane; iodide

1-Ethylsulfanylthiocarbonyl-2,8,9-trimethyl-2,5,8,9-tetraaza-1-phosphonia-bicyclo[3.3.3]undecane; iodide

Conditions
ConditionsYield
In acetonitrile for 0.366667h;100%
ethyl iodide
75-03-6

ethyl iodide

O,O-diethyltrimethylsilylchloromethylphosphonate α-lithie
176100-94-0

O,O-diethyltrimethylsilylchloromethylphosphonate α-lithie

(1-Chloro-1-trimethylsilanyl-propyl)-phosphonic acid diethyl ester
118512-68-8

(1-Chloro-1-trimethylsilanyl-propyl)-phosphonic acid diethyl ester

Conditions
ConditionsYield
In tetrahydrofuran; hexane for 1h; Ambient temperature;100%
ethyl iodide
75-03-6

ethyl iodide

4,6-dimethyl-1-phenyl-2-oxopyrimidine
21139-18-4

4,6-dimethyl-1-phenyl-2-oxopyrimidine

4-methyl-1-phenyl-6-propylpyrimidin-2(1H)-one
61404-63-5

4-methyl-1-phenyl-6-propylpyrimidin-2(1H)-one

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide for 1h;100%

75-03-6Upstream product

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