[Cyclohexylidene(phenylsulfanyl)methyl](trimethyl)silane

Base Information

Chemical Name:[Cyclohexylidene(phenylsulfanyl)methyl](trimethyl)silane
CAS No.:71342-13-7
Molecular Formula:C16H24SSi
Molecular Weight:276.518
Hs Code.:
DSSTox Substance ID:DTXSID70501074

Synonyms:71342-13-7;[Cyclohexylidene(phenylsulfanyl)methyl](trimethyl)silane;DTXSID70501074

Suppliers and Price of [Cyclohexylidene(phenylsulfanyl)methyl](trimethyl)silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Cyclohexylidene(phenylsulfanyl)methyl](trimethyl)silane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:276.13679847
Heavy Atom Count:18
Complexity:287

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C(=C1CCCCC1)SC2=CC=CC=C2

Technology Process of [Cyclohexylidene(phenylsulfanyl)methyl](trimethyl)silane

There total 1 articles about [Cyclohexylidene(phenylsulfanyl)methyl](trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 69190-57-4
<1,1-bis(phenylthio)methylene>cyclohexane

: 71342-13-7
trimethylsilane

Guidance literature:: Multistep reaction; (i) Li, naphthalene, (ii) /BRN= 1209232/;
DOI:10.1021/jo01334a041

Reference yield:

: 71342-13-7
trimethylsilane

: ((E)-2-Chloro-1,2-dicyclohexyl-vinyl)-trimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium 1-(dimethylamino)naphthalenide / 1.) 1 h, -45 deg C

2: SOCl₂ / CCl₄ / 2 h / 0 °C

With thionyl chloride; lithium 1-(dimethylamino)naphthalenide; In tetrachloromethane;
DOI:10.1021/ja00323a031

Reference yield:

: 71342-13-7
trimethylsilane

: 53723-46-9
trans-1-(1-cyclohexenyl)-2-cyclohexylethene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium 1-(dimethylamino)naphthalenide / 1.) 1 h, -45 deg C

2: SOCl₂ / CCl₄ / 2 h / 0 °C

3: tetra-n-butylammonium fluoride / tetrahydrofuran; dimethylsulfoxide / 1.5 h

With thionyl chloride; lithium 1-(dimethylamino)naphthalenide; tetrabutyl ammonium fluoride; In tetrahydrofuran; tetrachloromethane; dimethyl sulfoxide;
DOI:10.1021/ja00323a031