N-(6-cyanonaphthalen-2-yl)benzamide

Base Information

Chemical Name:N-(6-cyanonaphthalen-2-yl)benzamide
CAS No.:71590-35-7
Molecular Formula:C18H12N2O
Molecular Weight:272.30100
Hs Code.:
DSSTox Substance ID:DTXSID10457021
Wikidata:Q82279692
ChEMBL ID:CHEMBL109287

Synonyms:N-(6-cyanonaphthalen-2-yl)benzamide;71590-35-7;CHEMBL109287;SCHEMBL5561129;DTXSID10457021;BDBM50138672;N-(6-Carbamimidoyl-naphthalen-2-yl)-benzamide

Suppliers and Price of N-(6-cyanonaphthalen-2-yl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of N-(6-cyanonaphthalen-2-yl)benzamide

Chemical Property:

Boiling Point:410.9±18.0 °C(Predicted)
PSA：52.89000
Density:1.26±0.1 g/cm3(Predicted)
LogP:4.03678
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:272.094963011
Heavy Atom Count:21
Complexity:418

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)NC2=CC3=C(C=C2)C=C(C=C3)C#N

Technology Process of N-(6-cyanonaphthalen-2-yl)benzamide

There total 10 articles about N-(6-cyanonaphthalen-2-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 129667-70-5
6-amino-2-naphthalenecarbonitrile

: 98-88-4
benzoyl chloride

: 71590-35-7
2-Cyan-6-benzoylaminonaphthalen

Guidance literature:: With potassium carbonate; In 1,4-dioxane; at 20 ℃; for 0.166667h;
DOI:10.1021/jm0300072

Reference yield:

: 5159-60-4
6-cyano-naphthalene-2-carboxylic acid

: 71590-35-7
2-Cyan-6-benzoylaminonaphthalen

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / (COCl)2 / toluene / 22 h / 70 °C

2: 90 percent / NaN₃ / acetone / 1.5 h / 20 °C

3: 67 percent / H₂SO₄ / 1 h / 0 - 20 °C

4: 34 percent / aq. K₂CO₃ / dioxane / 0.17 h / 20 °C

With sodium azide; oxalyl dichloride; sulfuric acid; potassium carbonate; In 1,4-dioxane; acetone; toluene;
DOI:10.1021/jm0300072

Reference yield:

: 68635-22-3
6-Cyano-naphthalene-2-carbonyl chloride

: 71590-35-7
2-Cyan-6-benzoylaminonaphthalen

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / NaN₃ / acetone / 1.5 h / 20 °C

2: 67 percent / H₂SO₄ / 1 h / 0 - 20 °C

3: 34 percent / aq. K₂CO₃ / dioxane / 0.17 h / 20 °C

With sodium azide; sulfuric acid; potassium carbonate; In 1,4-dioxane; acetone;
DOI:10.1021/jm0300072