Technology Process of cis-4-Dodecene
There total 3 articles about cis-4-Dodecene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
1,4-dioxane; water;
for 3h;
Product distribution;
Heating;
various aliphatic and aromatic aldehydes, phosphonium salts; Wittig reaction, catalyzed with K2CO3, comparison with NaOH catalysis;
- Guidance literature:
-
Multi-step reaction with 2 steps
2: 1.) t-BuLi, 2.) HMPT / 1.) Et2O, pentane, -78 - (-50) deg C, 15 min, 2.) Et2O, propane, THF, -50 deg C - room temperature
With
N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium;
DOI:10.1080/00397919608004635
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium;
Yield given. Multistep reaction;
1.) Et2O, pentane, -78 - (-50) deg C, 15 min, 2.) Et2O, propane, THF, -50 deg C - room temperature;
DOI:10.1080/00397919608004635
