2-Pentenoic acid, 5-hydroxy-5-phenyl-, methyl ester, (2E)-

Base Information

Chemical Name:2-Pentenoic acid, 5-hydroxy-5-phenyl-, methyl ester, (2E)-
CAS No.:72853-47-5
Molecular Formula:C12H14O3
Molecular Weight:206.241
Hs Code.:

Synonyms:(+-)-1-Hydroxy-1-phenyl-penten-(3t)-saeure-(5)-methylester;methyl 5-hydroxy-5-phenyl-2-pentenoate;(E)-Methyl 5-hydroxy-5-phenyl-2-pentenoate;5-hydroxy-5-phenyl-pent-2-enoic acid methyl ester;2-Pentenoic acid,5-hydroxy-5-phenyl-,methyl ester,(2E);(+-)-1-hydroxy-1-phenyl-penten-(3t)-oic acid-(5)-methyl ester;

Suppliers and Price of 2-Pentenoic acid, 5-hydroxy-5-phenyl-, methyl ester, (2E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Pentenoic acid, 5-hydroxy-5-phenyl-, methyl ester, (2E)-

Chemical Property:

Boiling Point:339.8±42.0 °C(Predicted)
PSA：46.53000
Density:1.123±0.06 g/cm3(Predicted)
LogP:1.83930

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Pentenoic acid, 5-hydroxy-5-phenyl-, methyl ester, (2E)-

There total 13 articles about 2-Pentenoic acid, 5-hydroxy-5-phenyl-, methyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 80735-94-0,936-58-3
1-Phenyl-3-buten-1-ol

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 72853-47-5
5-hydroxy-5-phenyl-pent-2-enoic acid methyl ester

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; Inert atmosphere; Reflux;
DOI:10.1039/C6OB02333A

Reference yield: 97.0%

: 623-43-8
crotonic acid methyl ester

: 100-52-7
benzaldehyde

: 72853-47-5
5-hydroxy-5-phenyl-pent-2-enoic acid methyl ester

Guidance literature:: crotonic acid methyl ester; benzaldehyde; With aluminium tris(2,6-diphenylphenoxide); In toluene; at -78 ℃; for 0.333333h;

With 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; hexane; toluene; at -78 ℃; for 0.5h;
DOI:10.1002/(SICI)1521-3773(19990614)38:12<1769::AID-ANIE1769>3.0.CO;2-0

Reference yield: 72.0%

: 85636-50-6
1-(trimethylsiloxy)-1-methoxy-1,3-butadiene

: 100-52-7
benzaldehyde

: 72853-47-5
5-hydroxy-5-phenyl-pent-2-enoic acid methyl ester

Guidance literature:: With tetrabutylammonium triphenyldifluorosilicate; In tetrahydrofuran; at 20 ℃; for 6h;
DOI:10.1016/j.tetasy.2017.05.003