P,P-Dimethyl-N-(trimethylsilyl)phosphinimidic bromide

Base Information

• Chemical Name: P,P-Dimethyl-N-(trimethylsilyl)phosphinimidic bromide
• CAS No.: 73296-38-5
• Molecular Formula: C5H15BrNPSi
• Molecular Weight: 228.144
• DSSTox Substance ID: DTXSID80503923
• Nikkaji Number: J2.390.650C
• Wikidata: Q82358045

Synonyms:73296-38-5;P,P-Dimethyl-N-(trimethylsilyl)phosphinimidic bromide;DTXSID80503923

Chemical Property of P,P-Dimethyl-N-(trimethylsilyl)phosphinimidic bromide

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 226.98948
• Heavy Atom Count: 9
• Complexity: 144

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)N=P(C)(C)Br

Technology Process of P,P-Dimethyl-N-(trimethylsilyl)phosphinimidic bromide

There total 1 articles about P,P-Dimethyl-N-(trimethylsilyl)phosphinimidic bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Et3P*PMe2=NSiMe3]Br (1160553-30-9) + tris(pentafluorophenyl)borate (1109-15-5) → Et3P·B(C6F5)3 (1054577-37-5) + BrMe2P=NSiMe3 (73296-38-5)

Guidance literature:

In chloroform; for 36h; Inert atmosphere;

Reference yield:

tri-tert-butylphosphine oxide (6866-70-2) + BrMe2P=NSiMe3 (73296-38-5) → Br(1-)*C17H42NOP2Si(1+) (1335045-43-6)

Guidance literature:

In dichloromethane; at 25 ℃;

DOI:10.1021/ic201360p

Reference yield:

tri-tert-butylphosphine oxide (6866-70-2) + silver trifluoromethanesulfonate (2923-28-6) + BrMe2P=NSiMe3 (73296-38-5) → CF3O3S(1-)*C17H42NOP2Si(1+) (1335045-21-0)

Guidance literature:

In dichloromethane; at 25 ℃; for 16h;

DOI:10.1021/ic201360p

upstream raw materials:

[Et₃P*PMe₂=NSiMe₃]Br

tris(pentafluorophenyl)borate

Downstream raw materials:

2,2,4,4,6,6,8,8-octamethyl-2λ⁵,4λ⁵,6λ⁵,8λ⁵-cyclotetraphosphazene

hexamethylcyclotriphosphazene

[Me₂P=N]5

CF₃O₃S^(1-)*C₁₇H₄₂NOP₂Si⁽¹⁺⁾

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