2-[(4-Methylcyclohex-3-en-1-yl)methyl]oxolane

Base Information

Chemical Name:2-[(4-Methylcyclohex-3-en-1-yl)methyl]oxolane
CAS No.:73301-35-6
Molecular Formula:C12H20O
Molecular Weight:180.29
Hs Code.:
DSSTox Substance ID:DTXSID10502702

Synonyms:2-[(4-Methylcyclohex-3-en-1-yl)methyl]oxolane;73301-35-6;DTXSID10502702;AKOS024322073;2-[(4-METHYL-3-CYCLOHEXEN-1-YL)METHYL]TETRAHYDROFURAN

Suppliers and Price of 2-[(4-Methylcyclohex-3-en-1-yl)methyl]oxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 2-[(4-Methylcyclohex-3-en-1-yl)methyl]oxolane

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:180.151415257
Heavy Atom Count:13
Complexity:195

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CCC(CC1)CC2CCCO2

Technology Process of 2-[(4-Methylcyclohex-3-en-1-yl)methyl]oxolane

There total 4 articles about 2-[(4-Methylcyclohex-3-en-1-yl)methyl]oxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 73301-25-4
1-methyl-4-(2-tetrahydrofuryl)-4-(phenylsulfonyl)cyclohexene

: 73301-35-6
1-methyl-4-(2-tetrahydrofuryl)-cyclohexene

Guidance literature:: With sodium amalgam; Na₂HPO₄ buffer; In tetrahydrofuran; methanol; at -20 ℃;
DOI:10.1021/ja00522a075

Reference yield:

: 73301-15-2
1-phenylsulfonyl-4-methylcyclohex-3-ene

: 73301-35-6
1-methyl-4-(2-tetrahydrofuryl)-cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / tetrahydrofuran; hexamethylphosphoric acid triamide

2: 84 percent / 6percent sodium amalgam, Na₂HPO₄ buffer / methanol; tetrahydrofuran / -20 °C

With sodium amalgam; Na₂HPO₄ buffer; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/ja00522a075

Reference yield:

: 5831-70-9
2-(iodomethyl)tetrahydrofuran

: 73301-35-6
1-methyl-4-(2-tetrahydrofuryl)-cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / tetrahydrofuran; hexamethylphosphoric acid triamide

2: 84 percent / 6percent sodium amalgam, Na₂HPO₄ buffer / methanol; tetrahydrofuran / -20 °C

With sodium amalgam; Na₂HPO₄ buffer; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/ja00522a075