Benzaldehyde, 3-methoxy-4-nitro-2-(phenylmethoxy)-

Base Information

Chemical Name:Benzaldehyde, 3-methoxy-4-nitro-2-(phenylmethoxy)-
CAS No.:736137-85-2
Molecular Formula:C15H13NO5
Molecular Weight:287.272
Hs Code.:

Synonyms:

Suppliers and Price of Benzaldehyde, 3-methoxy-4-nitro-2-(phenylmethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzaldehyde, 3-methoxy-4-nitro-2-(phenylmethoxy)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 3-methoxy-4-nitro-2-(phenylmethoxy)-

There total 1 articles about Benzaldehyde, 3-methoxy-4-nitro-2-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 20041-61-6
2-hydroxy-3-methoxy-4-nitrobenzaldehyde

: 100-39-0
benzyl bromide

: 736137-85-2
2-benzyloxy-3-methoxy-4-nitrobenzaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 14h;
DOI:10.1021/ja064228j

Reference yield: 97.0%

: 736137-85-2
2-benzyloxy-3-methoxy-4-nitrobenzaldehyde

: 736137-86-3
2-benzyloxy-3-methoxy-4-nitrobenzoic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tert-butyl alcohol; at 25 ℃; for 2h;
DOI:10.1021/ja0472735

Reference yield:

: 736137-85-2
2-benzyloxy-3-methoxy-4-nitrobenzaldehyde

: 736137-87-4
2-benzyloxy-3-methoxy-4-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: 97 percent / aq. NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol / 12 h / 25 °C

2.1: diphenylphosphoryl azide; Et₃N / tetrahydrofuran / 3 h / 25 °C

2.2: 78 percent / H₂O / tetrahydrofuran / 2 h / Heating

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; diphenylphosphoranyl azide; triethylamine; In tetrahydrofuran; tert-butyl alcohol; 2.2: Curtius rearrangement;
DOI:10.1021/ja064228j