Silane, (1,1-dimethylethyl)dimethyl[(1-phenyl-2-propenyl)oxy]-

Base Information

Chemical Name:Silane, (1,1-dimethylethyl)dimethyl[(1-phenyl-2-propenyl)oxy]-
CAS No.:73795-12-7
Molecular Formula:C15H24OSi
Molecular Weight:248.44
Hs Code.:
DSSTox Substance ID:DTXSID70457320
Nikkaji Number:J1.485.581E

Synonyms:73795-12-7;Silane, (1,1-dimethylethyl)dimethyl[(1-phenyl-2-propenyl)oxy]-;DTXSID70457320;vinyl benzyl t-butyldimethylsilyl ether;1-(tert-Butyldimethylsiloxy)allylbenzene

Suppliers and Price of Silane, (1,1-dimethylethyl)dimethyl[(1-phenyl-2-propenyl)oxy]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Silane, (1,1-dimethylethyl)dimethyl[(1-phenyl-2-propenyl)oxy]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:248.159641919
Heavy Atom Count:17
Complexity:246

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C)(C)OC(C=C)C1=CC=CC=C1

Technology Process of Silane, (1,1-dimethylethyl)dimethyl[(1-phenyl-2-propenyl)oxy]-

There total 4 articles about Silane, (1,1-dimethylethyl)dimethyl[(1-phenyl-2-propenyl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 4393-06-0
1-Phenyl-2-propen-1-ol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 73795-12-7
1-phenylprop-2-en-1-yl tert-butyldimethylsilyl ether

Guidance literature:: With 1H-imidazole; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jo970435d

Reference yield: 76.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 2687-12-9
cinnamyl chloride

: 73795-12-7
1-phenylprop-2-en-1-yl tert-butyldimethylsilyl ether

Guidance literature:: cinnamyl chloride; With (η⁵-C5Me5)2-(Zr=O)-(4-(3-phenylpropyl)pyridin-1-yl); In benzene; at 45 ℃; for 8h;

t-butyldimethylsiyl triflate; In benzene; at 105 ℃; for 14h; Further stages.;
DOI:10.1021/ja075967i

Reference yield:

: 100-52-7
benzaldehyde

: 73795-12-7
1-phenylprop-2-en-1-yl tert-butyldimethylsilyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere

With 1H-imidazole; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol301026w