4-Amino-2,3-dimethylbenzene-1-sulfonic acid

Base Information

Chemical Name:4-Amino-2,3-dimethylbenzene-1-sulfonic acid
CAS No.:74319-86-1
Molecular Formula:C₈H₁₁NO₃S
Molecular Weight:201.246
Hs Code.:
DSSTox Substance ID:DTXSID30503271
Nikkaji Number:J1.800.565D
Wikidata:Q82356947

Synonyms:74319-86-1;p-Xylidinsulfosaure;SCHEMBL11689305;DTXSID30503271;4-Amino-2,3-dimethylbenzene-1-sulfonic acid

Suppliers and Price of 4-Amino-2,3-dimethylbenzene-1-sulfonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Amino-2,3-dimethylbenzene-1-sulfonic acid

Chemical Property:

XLogP3:0.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:201.04596439
Heavy Atom Count:13
Complexity:270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC(=C1C)S(=O)(=O)O)N

Technology Process of 4-Amino-2,3-dimethylbenzene-1-sulfonic acid

There total 11 articles about 4-Amino-2,3-dimethylbenzene-1-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 2,3-dimethylanilinium butylamidosulfate

: 80867-75-0
2-amino-3,4-dimethylbenzenesulfonic acid

: 74319-86-1
4-amino-2,3-dimethylbenzenesulfonic acid

: (2,3-dimethyl-phenyl)-amidosulfuric acid

: 4-Amino-5,6-dimethyl-benzene-1,3-disulfonic acid

Guidance literature:: at 140 ℃; for 8h; Further byproducts given;

Reference yield: 5.0%

: 2,3-dimethylanilinium butylamidosulfate

: 80867-75-0
2-amino-3,4-dimethylbenzenesulfonic acid

: 74319-86-1
4-amino-2,3-dimethylbenzenesulfonic acid

: 4-Amino-5,6-dimethyl-benzene-1,3-disulfonic acid

Guidance literature:: at 160 ℃; for 8h;

Reference yield:

: 80879-86-3
2,3-dimethyl-4-nitroaniline

: 74319-86-1
4-amino-2,3-dimethylbenzenesulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaNO₂, HCl, 2.) SO₂, CuCl₂

2: Na₂CO₃ / methanol / 1 h / Heating

3: Fe

With hydrogenchloride; sulfur dioxide; iron; sodium carbonate; copper dichloride; sodium nitrite; In methanol;