Heptanoic acid, 2,6-dimethyl-5-oxo-

Base Information

• Chemical Name: Heptanoic acid, 2,6-dimethyl-5-oxo-
• CAS No.: 74457-59-3
• Molecular Formula: C9H16O3
• Molecular Weight: 172.224
• Mol file: 74457-59-3.mol

Synonyms:

Chemical Property of Heptanoic acid, 2,6-dimethyl-5-oxo-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Heptanoic acid, 2,6-dimethyl-5-oxo-

There total 2 articles about Heptanoic acid, 2,6-dimethyl-5-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

2-hydroxy-1-p-menthen-3-one (490-03-9,468722-70-5) → 2-isopropyl-5-oxohexanoic acid (2543-54-6) + 2,6-dimethyl-5-oxo-heptanoic acid (74457-59-3) + 1,2-Dihydroxy-5-isopropyl-2-methyl-cyclopentanecarboxylic acid (74457-60-6)

Guidance literature:

With sodium hydroxide; oxygen; In water;

DOI:10.1016/S0040-4039(00)78839-3

Reference yield: 11.0%

2-hydroxy-1-p-menthen-3-one (490-03-9,468722-70-5) → 2-isopropyl-5-oxohexanoic acid (2543-54-6) + 2,6-dimethyl-5-oxo-heptanoic acid (74457-59-3)

Guidance literature:

With sodium hydroxide; oxygen; trimethyldodecylammonium chloride; In water; for 7h;

DOI:10.1016/S0040-4039(00)78839-3

Reference yield:

2,6-dimethyl-5-oxo-heptanoic acid (74457-59-3) → 2-methylglutaric acid (18069-17-5)

Guidance literature:

α-methyl-isobutyryl-butyric acid from dihydrocamphorphorone; bei weiterer Oxidation;

upstream raw materials:

2-hydroxy-1-p-menthen-3-one

Downstream raw materials:

2-methylglutaric acid

acetone

Bromoform

acetic acid

Refernces