1,3-Dioxolane, 2-[4-(bromomethyl)phenyl]-

Base Information

Chemical Name:1,3-Dioxolane, 2-[4-(bromomethyl)phenyl]-
CAS No.:74508-89-7
Molecular Formula:C10H11BrO2
Molecular Weight:243.1
Hs Code.:
DSSTox Substance ID:DTXSID70478252
Nikkaji Number:J2.771.959G
Wikidata:Q82311499

Synonyms:74508-89-7;1,3-Dioxolane, 2-[4-(bromomethyl)phenyl]-;SCHEMBL2237097;DTXSID70478252

Suppliers and Price of 1,3-Dioxolane, 2-[4-(bromomethyl)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,3-Dioxolane, 2-[4-(bromomethyl)phenyl]-

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:241.99424
Heavy Atom Count:13
Complexity:149

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC(O1)C2=CC=C(C=C2)CBr

Technology Process of 1,3-Dioxolane, 2-[4-(bromomethyl)phenyl]-

There total 3 articles about 1,3-Dioxolane, 2-[4-(bromomethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 51359-78-5
4-(bromomethyl)benzaldehyde

: 107-21-1
ethylene glycol

: 74508-89-7
2-(4-(bromomethyl)phenyl)-1,3-dioxolane

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 140 ℃; Dean-Stark;

Reference yield:

ether-petroleum ether: ether-petroleum ether

: 51359-78-5
4-(bromomethyl)benzaldehyde

: 74508-89-7
2-(4-(bromomethyl)phenyl)-1,3-dioxolane

Guidance literature:: With toluene-4-sulfonic acid; In ethylene glycol; benzene;

Reference yield:

: 17201-43-3
4-cyanobenzyl bromide

: 74508-89-7
2-(4-(bromomethyl)phenyl)-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / dichloromethane; hexane / 1 h / -70 - 0 °C / Inert atmosphere

2: toluene-4-sulfonic acid / toluene / 12 h / Reflux; Dean-Stark

With diisobutylaluminium hydride; toluene-4-sulfonic acid; In hexane; dichloromethane; toluene;
DOI:10.1002/ejoc.201600158