1H-Benzimidazole-1-acetic acid, 2,3-dihydro-5-chloro-2-oxo-3-phenyl-

Base Information

Chemical Name:1H-Benzimidazole-1-acetic acid, 2,3-dihydro-5-chloro-2-oxo-3-phenyl-
CAS No.:79759-53-8
Molecular Formula:C15H11ClN2O3
Molecular Weight:302.7124
Hs Code.:
DSSTox Substance ID:DTXSID60229876
Wikidata:Q83110244

Synonyms:BRN 5594182;79759-53-8;1H-Benzimidazole-1-acetic acid, 2,3-dihydro-5-chloro-2-oxo-3-phenyl-;2-Oxo-3-phenyl-5-chloro-benzimidazolin-1-yl-acetic acid;2,3-Dihydro-5-chloro-2-oxo-3-phenyl-1H-benzimidazole-1-acetic acid;(5-Chloro-2-oxo-3-phenyl-2,3-dihydro-1H-benzimidazol-1-yl)acetic acid;C15H11ClN2O3;DTXSID60229876;C15-H11-Cl-N2-O3;LS-32589

Suppliers and Price of 1H-Benzimidazole-1-acetic acid, 2,3-dihydro-5-chloro-2-oxo-3-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1H-Benzimidazole-1-acetic acid, 2,3-dihydro-5-chloro-2-oxo-3-phenyl-

Chemical Property:

Vapor Pressure:1.01E-11mmHg at 25°C
Boiling Point:522°Cat760mmHg
Flash Point:269.5°C
Density:1.473g/cm³
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:302.0458199
Heavy Atom Count:21
Complexity:425

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C3=C(C=CC(=C3)Cl)N(C2=O)CC(=O)O

Technology Process of 1H-Benzimidazole-1-acetic acid, 2,3-dihydro-5-chloro-2-oxo-3-phenyl-

There total 4 articles about 1H-Benzimidazole-1-acetic acid, 2,3-dihydro-5-chloro-2-oxo-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 79759-36-7
(5-Chloro-2-oxo-3-phenyl-2,3-dihydro-benzoimidazol-1-yl)-acetic acid ethyl ester

: 79759-53-8
2-oxo-3-phenyl-5-chloro-benzimidazolin-1-yl-acetic acid

Guidance literature:: With sodium hydroxide; In ethanol; at 50 ℃; for 0.5h;

Reference yield:

: 68406-47-3
4-chloro-N₂-phenylbenzene-1,2-diamine

: 79759-53-8
2-oxo-3-phenyl-5-chloro-benzimidazolin-1-yl-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / CHCl₃ / 20 h / Heating

2: 99.3 percent / EtONa / ethanol / 3 h / Heating

3: 34 percent / NaOH / methanol / 5 h / Heating

4: 73 percent / 2 N aq. NaOH / ethanol / 0.5 h / 50 °C

With sodium hydroxide; sodium ethanolate; In methanol; ethanol; chloroform;

Reference yield:

: 79759-11-8
N¹-phenyl-N²-carbethoxy-5-chloro-o.phenylenediamine

: 79759-53-8
2-oxo-3-phenyl-5-chloro-benzimidazolin-1-yl-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 99.3 percent / EtONa / ethanol / 3 h / Heating

2: 34 percent / NaOH / methanol / 5 h / Heating

3: 73 percent / 2 N aq. NaOH / ethanol / 0.5 h / 50 °C

With sodium hydroxide; sodium ethanolate; In methanol; ethanol;