N-Methyl-2,2-bis(4-chlorophenyl)acetamide

Base Information

• Chemical Name: N-Methyl-2,2-bis(4-chlorophenyl)acetamide
• CAS No.: 6316-74-1
• Molecular Formula: C₁₅H₁₃Cl₂NO
• Molecular Weight: 294.18
• NSC Number: 22503
• DSSTox Substance ID: DTXSID80979144
• Nikkaji Number: J2.889.718I
• Wikidata: Q82964683

Synonyms:6316-74-1;NSC22503;N-Methyl-2,2-bis(4-chlorophenyl)acetamide;SCHEMBL1978851;DTXSID80979144;NSC-22503;2,2-Bis(4-chlorophenyl)-N-methylethanimidic acid

Chemical Property of N-Methyl-2,2-bis(4-chlorophenyl)acetamide

Chemical Property:

• Vapor Pressure: 1.27E-09mmHg at 25°C
• Boiling Point: 486.7°C at 760 mmHg
• Flash Point: 248.1°C
• Density: 1.265g/cm³
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 293.0374194
• Heavy Atom Count: 19
• Complexity: 273

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CNC(=O)C(C1=CC=C(C=C1)Cl)C2=CC=C(C=C2)Cl

Technology Process of N-Methyl-2,2-bis(4-chlorophenyl)acetamide

There total 2 articles about N-Methyl-2,2-bis(4-chlorophenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-bis(4-chlorophenyl)acetyl chloride (68668-89-3) + methylamine (74-89-5) → bis-(4-chloro-phenyl)-acetic acid methylamide (6316-74-1)

Guidance literature:

With benzene;

Reference yield:

→ 2-(4-chloro-phenyl)-N-methyl-2-[4-(3-methyl-1-trityl-1H-pyrazol-4-yl)-phenyl]-acetamide (857532-36-6) + bis-(4-chloro-phenyl)-acetic acid methylamide (6316-74-1)

Guidance literature:

Reference yield:

bis-(4-chloro-phenyl)-acetic acid methylamide (6316-74-1) + triethyloxonium fluoroborate (368-39-8) → C17H17Cl2NO*BF4(1-)*H(1+)

Guidance literature:

With sodium carbonate; In dichloromethane; for 15h; Ambient temperature;

DOI:10.1021/jm00149a031

upstream raw materials:

2,2-bis(4-chlorophenyl)acetyl chloride

methylamine

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