Tris(3-chlorophenyl)boroxin

Base Information

Chemical Name:Tris(3-chlorophenyl)boroxin
CAS No.:7519-92-8
Molecular Formula:C18H12B3Cl3O3
Molecular Weight:415.083
Hs Code.:
DSSTox Substance ID:DTXSID201310082
Nikkaji Number:J1.957.669H

Synonyms:Tris(3-chlorophenyl)boroxin;SCHEMBL7858638;DTXSID201310082;2,4,6-Tris(3-chlorophenyl)boroxin;7519-92-8

Suppliers and Price of Tris(3-chlorophenyl)boroxin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Tris(3-chlorophenyl)boroxin

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:414.013118
Heavy Atom Count:27
Complexity:413

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B1(OB(OB(O1)C2=CC(=CC=C2)Cl)C3=CC(=CC=C3)Cl)C4=CC(=CC=C4)Cl

Technology Process of Tris(3-chlorophenyl)boroxin

There total 4 articles about Tris(3-chlorophenyl)boroxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63503-60-6
3-chlorophenylboronic acid

: 7519-92-8
tris(3-chlorophenyl)boroxine

Guidance literature:: at 110 ℃;
DOI:10.1021/ja01639a023

Reference yield:

: 7637-07-2
boron trifluoride

: 36229-42-2
(3-chlorophenyl)magnesium bromide

: 7519-92-8
tris(3-chlorophenyl)boroxine

Guidance literature:: byproducts: H2O; dehydration in a desiccator over H2SO4;;
DOI:10.1021/ja01140a021

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 36229-42-2
(3-chlorophenyl)magnesium bromide

: 7519-92-8
tris(3-chlorophenyl)boroxine

Guidance literature:: With sulfuric acid; In tetrahydrofuran; diethyl ether; byproducts: H2O; react. at -70°C in THF/ether, hydrolysis with ice/H2SO4, extractn. with ether, removal of ether, dehydration of residue on heating to 110°C;;
DOI:10.1039/j39660000566