3-Pentanone, 1,5-diphenyl-, O,O'-methylenedioxime

Base Information

Chemical Name:3-Pentanone, 1,5-diphenyl-, O,O'-methylenedioxime
CAS No.:75498-69-0
Molecular Formula:C₃₅H₃₈N₂O₂
Molecular Weight:518.699
Hs Code.:

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Chemical Property of 3-Pentanone, 1,5-diphenyl-, O,O'-methylenedioxime

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Technology Process of 3-Pentanone, 1,5-diphenyl-, O,O'-methylenedioxime

There total 2 articles about 3-Pentanone, 1,5-diphenyl-, O,O'-methylenedioxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 75-09-2
dichloromethane

: 5434-81-1
1,5-diphenyl-pentan-3-one oxime

: 75498-69-0
1,5-Diphenyl-pentan-3-one O-(1-phenethyl-3-phenyl-propylideneaminooxymethyl)-oxime

Guidance literature:: With KO₂; (2-methylallyl)palladium-chloride dimer; for 72h; Ambient temperature;
DOI:10.1016/S0040-4039(00)71386-4

Reference yield: 27.0%

: (2-methylallyl)palladium-chloride dimer

: 5434-81-1
1,5-diphenyl-pentan-3-one oxime

: 2(C₆H₅CH₂CH₂)2CNO^(1-)*2(C₆H₅CH₂CH₂)2CNOH*Pd⁽²⁺⁾=[((C₆H₅CH₂CH₂)2CNO)2((C₆H₅CH₂CH₂)2CNOH)2]Pd

: 75498-69-0
1,5-Diphenyl-pentan-3-one O-(1-phenethyl-3-phenyl-propylideneaminooxymethyl)-oxime

Guidance literature:: With dichloromethane; In dichloromethane; byproducts: potassium chloride; KO2, Pd complex and ketoxime stirred in CH2Cl2 soln. for 72 h at room temp. under Ar; KCl filtered off, concd. in vac., chromd. (Al2O3, hexane-EtOAc, EtOAc, CH2Cl2), recrystd. from CH2Cl2-EtOAc; elem. anal.;
DOI:10.1246/bcsj.58.194