PROPANEDIOIC ACID, 2-(2-NITRO-1-PHENYLETHYL)-, 1,3-DIETHYL ESTER

Base Information

Chemical Name:PROPANEDIOIC ACID, 2-(2-NITRO-1-PHENYLETHYL)-, 1,3-DIETHYL ESTER
CAS No.:22975-21-9
Molecular Formula:C15H19NO6
Molecular Weight:309.3145
Hs Code.:
Mol file:22975-21-9.mol

Synonyms:HMS2601M15;diethyl 2-(2-nitro-1-phenylethyl)malonate;CL 520;

Suppliers and Price of PROPANEDIOIC ACID, 2-(2-NITRO-1-PHENYLETHYL)-, 1,3-DIETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DIETHYL 2-(2-NITRO-1-PHENYLETHYL)MALONATE 95.00%
1MG
$ 586.97

Total 6 raw suppliers

Chemical Property of PROPANEDIOIC ACID, 2-(2-NITRO-1-PHENYLETHYL)-, 1,3-DIETHYL ESTER

Chemical Property:

Vapor Pressure:1.12E-07mmHg at 25°C
Boiling Point:432.3°Cat760mmHg
Flash Point:171.8°C
PSA：98.42000
Density:1.195g/cm³
LogP:2.31250

Purity/Quality:

99% ^*data from raw suppliers

DIETHYL 2-(2-NITRO-1-PHENYLETHYL)MALONATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of PROPANEDIOIC ACID, 2-(2-NITRO-1-PHENYLETHYL)-, 1,3-DIETHYL ESTER

There total 32 articles about PROPANEDIOIC ACID, 2-(2-NITRO-1-PHENYLETHYL)-, 1,3-DIETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 5153-67-3
nitrostyrene

: 105-53-3
diethyl malonate

: 71639-13-9,22975-21-9
diethyl 2-(3-nitrophenylethyl)malonate

Guidance literature:: With lithium phenolate; (S)-3,3′-bis[hydroxy(diphenyl)methyl]-1,1′-binaphthalene-2,2′-diol; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.tetasy.2010.12.003

Reference yield: 99.0%

: 102-96-5
(2-nitroethenyl)benzene

: 105-53-3
diethyl malonate

: 22975-21-9
(R)-1,3-diethyl 2-(2-nitro-1-phenylethyl)malonate

Guidance literature:: With poly((1S,2S)-N¹,N²-bis(4-hydrooxybenzyl)cyclohexane-1,2-diamine naphthalene-2,7-disulfate (diester)), complex with NiBr₂; In dichloromethane; at 20 ℃; for 24h; Solvent; enantioselective reaction; Catalytic behavior;
DOI:10.1016/j.tetlet.2020.152792

Reference yield: 99.0%

: 102-96-5
(2-nitroethenyl)benzene

: 105-53-3
diethyl malonate

: 252338-27-5,22975-21-9
ethyl (S)-2-ethoxycarbonyl-4-nitro-3-phenylbutyrate

Guidance literature:: With 1-(3,5-bis(trifluoromethyl)benzyl)-3-((1S,2S)-2-(dimethylamino)cyclohexyl)thiourea; In toluene; at 20 ℃; enantioselective reaction;
DOI:10.1002/anie.201601028