N,N-diethyl-2-iodobenzamide

Base Information

Chemical Name:N,N-diethyl-2-iodobenzamide
CAS No.:76041-87-7
Molecular Formula:C11H14INO
Molecular Weight:303.143
Hs Code.:
DSSTox Substance ID:DTXSID401310745
Nikkaji Number:J1.123.182I

Synonyms:N,N-diethyl-2-iodobenzamide;76041-87-7;2-Iodo-N,N-diethylbenzamide;SCHEMBL10488519;DTXSID401310745;BDA04187;AKOS003235448;BS-32774;CS-0212919;SR-01000216010;SR-01000216010-1

Suppliers and Price of N,N-diethyl-2-iodobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N,N-Diethyl-2-iodobenzamide
500mg
$ 280.00

American Custom Chemicals Corporation
N,N-DIETHYL-2-IODOBENZAMIDE 95.00%
5MG
$ 498.41

Total 5 raw suppliers

Chemical Property of N,N-diethyl-2-iodobenzamide

Chemical Property:

PSA：20.31000
LogP:2.77320
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:303.01201
Heavy Atom Count:14
Complexity:192

Purity/Quality:

99% ^*data from raw suppliers

N,N-Diethyl-2-iodobenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=CC=CC=C1I

Technology Process of N,N-diethyl-2-iodobenzamide

There total 5 articles about N,N-diethyl-2-iodobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1696-17-9
N,N-diethylbenzamide

: 76041-87-7
N,N-diethyl-2-iodobenzamide

Guidance literature:: N,N-diethylbenzamide; With (2,2,6,6-tetramethylpiperidido)₂Ag(CN)Li₂; In tetrahydrofuran; at 0 ℃; for 2h;

With iodine; In tetrahydrofuran; at 20 ℃; for 3h; chemoselective reaction;
DOI:10.1039/c9sc06060j

Reference yield: 93.0%

: 609-67-6
2-Iodobenzoyl chloride

: 109-89-7
diethylamine

: 76041-87-7
N,N-diethyl-2-iodobenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 5h;
DOI:10.1021/jo402776u

Reference yield: 83.0%

: 88-67-5
2-Iodobenzoic acid

: 109-89-7
diethylamine

: 76041-87-7
N,N-diethyl-2-iodobenzamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 120h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.12.094