Technology Process of Benzenamine, 2-(1,3-dithian-2-yl)-4,5-dimethoxy-
There total 2 articles about Benzenamine, 2-(1,3-dithian-2-yl)-4,5-dimethoxy- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium chloride; iron;
In
ethanol; water;
for 3.5h;
Heating;
DOI:10.1021/jo049344o
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / boron trifluoride etherate; acetic acid / toluene
2: 81 percent / iron; ammonium chloride / H2O; ethanol / 3.5 h / Heating
With
boron trifluoride diethyl etherate; ammonium chloride; iron; acetic acid;
In
ethanol; water; toluene;
DOI:10.1021/jo049344o
- Guidance literature:
-
2-(4',5'-dimethoxy-2'-aminophenyl)-1,3-dithiane;
With
hydrogenchloride; sodium nitrite;
In
water;
at 0 - 5 ℃;
for 0.5h;
With
potassium ethyl xanthogenate;
In
water;
at 40 - 45 ℃;
for 0.833333h;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 2h;
DOI:10.1021/jo049344o
