1,2-Ethanediol, 1-phenyl-, dibenzoate

Base Information

• Chemical Name: 1,2-Ethanediol, 1-phenyl-, dibenzoate
• CAS No.: 7717-61-5
• Molecular Formula: C22H18O4
• Molecular Weight: 346.383
• Mol file: 7717-61-5.mol

Synonyms:1,2-bis-benzoyloxy-1-phenyl-ethane;1,2-Bis-benzoyloxy-1-phenyl-aethan;2-Phenylglycol Dibenzoate;Phenylethylenglycol-dibenzoat;1-Phenyl-1,2-aethandiol-dibenzoat;11.12-Dibenzoyloxy-1-aethyl-benzol;1-Phenylethylen-dibenzoat;1,2-Ethanediol,1-phenyl-,dibenzoate;

Chemical Property of 1,2-Ethanediol, 1-phenyl-, dibenzoate

Chemical Property:

• PSA: 115.06000
• LogP: 3.48190

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2-Ethanediol, 1-phenyl-, dibenzoate

There total 19 articles about 1,2-Ethanediol, 1-phenyl-, dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

phenylethane 1,2-diol (93-56-1) + benzoyl chloride (98-88-4) → 1-phenylethane-1,2-diyl dibenzoate (7717-61-5)

Guidance literature:

With triethylamine; for 24h; Ambient temperature;

Reference yield: 83.0%

phenylethane 1,2-diol (93-56-1) + N-benzoyloxybenzotriazole (54769-36-7) → 2-hydroxy-2-phenylethyl benzoate (10335-95-2) + 1-phenylethane-1,2-diyl dibenzoate (7717-61-5) + 2-hydroxy-1-phenylethyl benzoate (53574-78-0)

Guidance literature:

With triethylamine; In dichloromethane; for 24h; Product distribution; Ambient temperature; other diols;

DOI:10.1021/jo00210a036

Reference yield: 82.0%

1-benzoylimidazole (10364-94-0) + phenylethane 1,2-diol (93-56-1) → 2-hydroxy-2-phenylethyl benzoate (10335-95-2) + 1-phenylethane-1,2-diyl dibenzoate (7717-61-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 50 ℃; for 8h; regioselective reaction;

DOI:10.3390/molecules21050641

upstream raw materials:

styrene

silver benzoate

dibenzoyl peroxide

2-iodo-1-phenylethyl benzoate