N-[(1-Oxo-1lambda~5~-pyridin-4-yl)methyl]-2-phenylacetamide

Base Information

Chemical Name:N-[(1-Oxo-1lambda~5~-pyridin-4-yl)methyl]-2-phenylacetamide
CAS No.:77502-54-6
Molecular Formula:C14H14N2O2
Molecular Weight:242.277
Hs Code.:
DSSTox Substance ID:DTXSID30512242
Wikidata:Q82371406

Synonyms:77502-54-6;DTXSID30512242;N-[(1-Oxo-1lambda~5~-pyridin-4-yl)methyl]-2-phenylacetamide

Suppliers and Price of N-[(1-Oxo-1lambda~5~-pyridin-4-yl)methyl]-2-phenylacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(1-Oxo-1lambda~5~-pyridin-4-yl)methyl]-2-phenylacetamide

Chemical Property:

XLogP3:0.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:242.105527694
Heavy Atom Count:18
Complexity:257

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CC(=O)NCC2=CC=[N+](C=C2)[O-]

Technology Process of N-[(1-Oxo-1lambda~5~-pyridin-4-yl)methyl]-2-phenylacetamide

There total 3 articles about N-[(1-Oxo-1lambda~5~-pyridin-4-yl)methyl]-2-phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 80818-98-0
2-phenyl-N-(pyridin-4-ylmethyl)acetamide

: 77502-54-6
N-(1-Oxy-pyridin-4-ylmethyl)-2-phenyl-acetamide

Guidance literature:: With dihydrogen peroxide; In acetic acid; at 80 ℃;
DOI:10.1002/jhet.5570180707

Reference yield:

: 3731-53-1
4-(aminomethyl)pyridine

: 77502-54-6
N-(1-Oxy-pyridin-4-ylmethyl)-2-phenyl-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexylcarbodiimide / acetonitrile / 24 h / Ambient temperature

2: 73 percent / hydrogen peroxide (40 percent) / acetic acid / 80 °C

With dihydrogen peroxide; dicyclohexyl-carbodiimide; In acetic acid; acetonitrile;
DOI:10.1002/jhet.5570180707

Reference yield:

: 103-82-2
phenylacetic acid

: 77502-54-6
N-(1-Oxy-pyridin-4-ylmethyl)-2-phenyl-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexylcarbodiimide / acetonitrile / 24 h / Ambient temperature

2: 73 percent / hydrogen peroxide (40 percent) / acetic acid / 80 °C

With dihydrogen peroxide; dicyclohexyl-carbodiimide; In acetic acid; acetonitrile;
DOI:10.1002/jhet.5570180707