N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bisbenzeneacetamide

Base Information

Chemical Name:N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bisbenzeneacetamide
CAS No.:77502-38-6
Molecular Formula:C28H26 N4 O2
Molecular Weight:0
Hs Code.:2933399090
DSSTox Substance ID:DTXSID50998701
Mol file:77502-38-6.mol

Synonyms:77502-38-6;N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bisbenzeneacetamide;Benzeneacetamide, N,N'-(1,2-di-4-pyridinyl-1,2-ethanediyl)bis-;N,N'-[1,2-Di(4-pyridinyl)-1,2-ethanediyl]bis(2-phenylacetamide);DTXSID50998701;LS-28539;N,N'-[1,2-Di(pyridin-4-yl)ethane-1,2-diyl]bis(2-phenylethanimidic acid)

Suppliers and Price of N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bisbenzeneacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bisbenzeneacetamide

Chemical Property:

Boiling Point:771.8oC at 760 mmHg
Flash Point:420.6oC
PSA：90.96000
Density:1.216g/cm3
LogP:5.65740
XLogP3:3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:450.20557608
Heavy Atom Count:34
Complexity:564

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CC(=O)NC(C2=CC=NC=C2)C(C3=CC=NC=C3)NC(=O)CC4=CC=CC=C4

Technology Process of N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bisbenzeneacetamide

There total 4 articles about N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bisbenzeneacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 80818-98-0
2-phenyl-N-(pyridin-4-ylmethyl)acetamide

: 77502-54-6
N-(1-Oxy-pyridin-4-ylmethyl)-2-phenyl-acetamide

: 77502-38-6
2-Phenyl-N-(2-phenylacetylamino-1,2-di-pyridin-4-yl-ethyl)-acetamide

Guidance literature:: With acetic anhydride; at 70 ℃; for 3h;
DOI:10.1002/jhet.5570200658

Reference yield: 22.0%

: 77502-54-6
N-(1-Oxy-pyridin-4-ylmethyl)-2-phenyl-acetamide

: 77502-38-6
2-Phenyl-N-(2-phenylacetylamino-1,2-di-pyridin-4-yl-ethyl)-acetamide

Guidance literature:: In acetic anhydride; at 140 ℃; for 1.5h;
DOI:10.1002/jhet.5570180707

Reference yield:

: 3731-53-1
4-(aminomethyl)pyridine

: 77502-38-6
2-Phenyl-N-(2-phenylacetylamino-1,2-di-pyridin-4-yl-ethyl)-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide / acetonitrile / 24 h / Ambient temperature

2: 73 percent / hydrogen peroxide (40 percent) / acetic acid / 80 °C

3: 22 percent / acetic anhydride / 1.5 h / 140 °C

With dihydrogen peroxide; dicyclohexyl-carbodiimide; In acetic anhydride; acetic acid; acetonitrile;
DOI:10.1002/jhet.5570180707