N,N-Diethyl-3-(pyridine-2-carbonyl)pyridine-2-carboxamide

Base Information

Chemical Name:N,N-Diethyl-3-(pyridine-2-carbonyl)pyridine-2-carboxamide
CAS No.:77924-12-0
Molecular Formula:C₁₆H₁₇N₃O₂
Molecular Weight:283.33
Hs Code.:
DSSTox Substance ID:DTXSID70506362
Wikidata:Q82362073

Synonyms:77924-12-0;N,N-Diethyl-3-(pyridine-2-carbonyl)pyridine-2-carboxamide;SCHEMBL16535088;DTXSID70506362;N,N-diethyl-3-(2-pyridinecarbonyl)-2-pyridinecarboxamide

Suppliers and Price of N,N-Diethyl-3-(pyridine-2-carbonyl)pyridine-2-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N,N-Diethyl-3-(pyridine-2-carbonyl)pyridine-2-carboxamide

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:283.132076794
Heavy Atom Count:21
Complexity:369

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=C(C=CC=N1)C(=O)C2=CC=CC=N2

Technology Process of N,N-Diethyl-3-(pyridine-2-carbonyl)pyridine-2-carboxamide

There total 2 articles about N,N-Diethyl-3-(pyridine-2-carbonyl)pyridine-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 7606-13-5
N,N-diethyl-2-pyridinecarboxamide

: 77924-12-0
N,N-Diethyl-3-(2-pyridinecarbonyl)-2-pyridinecarboxamide

: N,N-diethyl-3-(α-hydroxybenzyl)pyridine-2-carboxamide

Guidance literature:: With sec.-butyllithium; In tetrahydrofuran; at -78 ℃; for 2h; Title compound not separated from byproducts;
DOI:10.1016/0040-4020(94)01004-J

Reference yield:

: 100-52-7
benzaldehyde

: 7606-13-5
N,N-diethyl-2-pyridinecarboxamide

: 104084-48-2
1-phenylfuro<3,4-b>pyridine-3(1H)-one

: 77924-12-0
N,N-Diethyl-3-(2-pyridinecarbonyl)-2-pyridinecarboxamide

: N,N,N',N'-tetraethyl-2,3'-bipyridine-2',6-dicarboxamide

Guidance literature:: With sec.-butyllithium; silica gel; Yield given. Multistep reaction. Title compound not separated from byproducts; 1.) THF, -78 deg C, 2 h, 2.) CH₂Cl₂ (chromatography);
DOI:10.1016/0040-4020(94)01004-J