Ethanol, 2,2'-[3-(4-methoxyphenyl)-2-triazenylidene]bis-

Base Information

• Chemical Name: Ethanol, 2,2'-[3-(4-methoxyphenyl)-2-triazenylidene]bis-
• CAS No.: 78002-80-9
• Molecular Formula: C11H17N3O3
• Mol file: 78002-80-9.mol

Synonyms:

Chemical Property of Ethanol, 2,2'-[3-(4-methoxyphenyl)-2-triazenylidene]bis-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanol, 2,2'-[3-(4-methoxyphenyl)-2-triazenylidene]bis-

There total 1 articles about Ethanol, 2,2'-[3-(4-methoxyphenyl)-2-triazenylidene]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-aniline (104-94-9) + 2,2'-iminobis[ethanol] (111-42-2) → C11H17N3O3 (78002-80-9)

Guidance literature:

4-methoxy-aniline; With potassium hydroxide; sodium nitrite; In water; for 0.166667h; Cooling with ice;

2,2'-iminobis[ethanol]; In water; for 0.5h; Cooling with ice;

DOI:10.1039/c4cc08367a

Reference yield: 49.0%

benzyl chloride (100-44-7) + C11H17N3O3 (78002-80-9) → 1-benzylsulfanyl-4-methoxy-benzene (26905-24-8)

Guidance literature:

benzyl chloride; With [2,2]bipyridinyl; copper(ll) sulfate pentahydrate; Sodium thiosulfate pentahydrate; In water; at 80 ℃; for 2h; Schlenk technique;

C₁₁H₁₇N₃O₃; With boron trifluoride diethyl etherate; In water; at 20 ℃; for 6h; Schlenk technique;

DOI:10.1039/c4cc08367a

upstream raw materials:

4-methoxy-aniline

2,2'-iminobis[ethanol]

Downstream raw materials:

1-benzylsulfanyl-4-methoxy-benzene

Refernces