4-[(ETHOXYCARBONYL)AMINO]BENZOIC ACID

Base Information

• Chemical Name: 4-[(ETHOXYCARBONYL)AMINO]BENZOIC ACID
• CAS No.: 5180-75-6
• Molecular Formula: C10H11 N O4
• Molecular Weight: 209.202
• Hs Code.: 2924299090
• Mol file: 5180-75-6.mol

Synonyms:Carbanilic acid, p-carboxy-,1-ethyl ester (7CI); Carbanilic acid, p-carboxy-, N-ethyl ester (6CI,8CI); 4-Carboxyphenylurethane;4-[(Ethoxycarbonyl)amino]benzoic acid

Chemical Property of 4-[(ETHOXYCARBONYL)AMINO]BENZOIC ACID

Chemical Property:

• Vapor Pressure: 0.00013mmHg at 25°C
• Boiling Point: 320.6°C at 760 mmHg
• Flash Point: 147.7°C
• PSA: 78.46000
• Density: 1.324g/cm³
• LogP: 0.69150
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

4-(Ethoxycarbonylamino)benzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-[(ETHOXYCARBONYL)AMINO]BENZOIC ACID

There total 10 articles about 4-[(ETHOXYCARBONYL)AMINO]BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

chloroformic acid ethyl ester (541-41-3) + 4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → 4-[(ethoxycarbonyl)amino]benzoic acid (5180-75-6)

Guidance literature:

chloroformic acid ethyl ester; 4-amino-benzoic acid; With TEA; In tetrahydrofuran; at 20 ℃; for 1h;

With trifluoroacetic acid; for 1h; Heating;

DOI:10.1016/j.tet.2006.09.103

Reference yield: 59.0%

ethyl 2-oxopyridin-1(2H)-yl carbonate (1425322-24-2) + 4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → 4-[(ethoxycarbonyl)amino]benzoic acid (5180-75-6)

Guidance literature:

With sodium carbonate; In water; acetone; at 0 - 20 ℃;

DOI:10.3390/molecules171214361

Reference yield: 43.0%

ethyl 2-cyano-2-(ethoxycarbonyloxyimino)acetate (41844-51-3) + 4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) → 4-[(ethoxycarbonyl)amino]benzoic acid (5180-75-6)

Guidance literature:

With sodium carbonate; In water; acetone; at 0 - 20 ℃;

DOI:10.3390/molecules171214361

upstream raw materials:

chloroformic acid ethyl ester

4-amino-benzoic acid

diethyl dicarbonate

ethanol

Downstream raw materials:

3-(4-aminophenyl)-3-oxopropanenitrile

4-ethoxycarbonylamino-benzoyl chloride

oxiran-2-ylmethyl 4-[(ethoxycarbonyl)amino]benzoate

4-ethoxycarbonylamino-benzoic acid methyl ester

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