1,1'-[(Difluoromethylene)disulfanediyl]bis(4-chlorobenzene)

Base Information

Chemical Name:1,1'-[(Difluoromethylene)disulfanediyl]bis(4-chlorobenzene)
CAS No.:78840-51-4
Molecular Formula:C13H8Cl2F2S2
Molecular Weight:337.241
Hs Code.:
DSSTox Substance ID:DTXSID10506346
Nikkaji Number:J1.298.014K
Wikidata:Q82362051

Synonyms:78840-51-4;DTXSID10506346;1,1'-[(Difluoromethylene)disulfanediyl]bis(4-chlorobenzene)

Suppliers and Price of 1,1'-[(Difluoromethylene)disulfanediyl]bis(4-chlorobenzene)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,1'-[(Difluoromethylene)disulfanediyl]bis(4-chlorobenzene)

Chemical Property:

XLogP3:6.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:335.9412543
Heavy Atom Count:19
Complexity:250

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1SC(F)(F)SC2=CC=C(C=C2)Cl)Cl

Technology Process of 1,1'-[(Difluoromethylene)disulfanediyl]bis(4-chlorobenzene)

There total 6 articles about 1,1'-[(Difluoromethylene)disulfanediyl]bis(4-chlorobenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1184-76-5
difluorodiiodomethane

: 106-54-7
p-Chlorothiophenol

: 1142-19-4
4,4'-dichlorodiphenyl disulfide

: 2488-66-6
1-chloro-4-[(difluoromethyl)sulfanyl]benzene

: 78840-51-4
difluorobis(4-chlorophenylthio)methane

: 272788-39-3
1-chloro-4-(difluoroiodomethylsulfanyl)benzene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 5h; Further Variations:; Reagents; Solvents; ratio of reagents; Product distribution;
DOI:10.1016/S0022-1139(99)00228-6

Reference yield: 65.0%

: 106-54-7
p-Chlorothiophenol

: 272788-39-3
1-chloro-4-(difluoroiodomethylsulfanyl)benzene

: 78840-51-4
difluorobis(4-chlorophenylthio)methane

Guidance literature:: p-Chlorothiophenol; With sodium hydride; In N,N-dimethyl-formamide; for 1h;

1-chloro-4-(difluoroiodomethylsulfanyl)benzene; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1016/S0022-1139(99)00228-6

Reference yield:

: 78840-52-5
1-{[bromo(difluoro)methyl]sulfanyl}-4-chlorobenzenenzene

: 78840-51-4
difluorobis(4-chlorophenylthio)methane

Guidance literature:: With silver hexafluoroantimonate; In dichloromethane; at -78 ℃; for 0.666667h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol402631t