2-(2,6,6-Trimethylcyclohex-2-en-1-yl)-1,3-dioxolane

Base Information

Chemical Name:2-(2,6,6-Trimethylcyclohex-2-en-1-yl)-1,3-dioxolane
CAS No.:78842-54-3
Molecular Formula:C12H20O2
Molecular Weight:196.29
Hs Code.:
DSSTox Substance ID:DTXSID40572438
Nikkaji Number:J996.200J

Synonyms:2-(2,6,6-Trimethylcyclohex-2-en-1-yl)-1,3-dioxolane;78842-54-3;SCHEMBL699489;DTXSID40572438

Suppliers and Price of 2-(2,6,6-Trimethylcyclohex-2-en-1-yl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-(2,6,6-Trimethylcyclohex-2-en-1-yl)-1,3-dioxolane

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:196.146329876
Heavy Atom Count:14
Complexity:237

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CCCC(C1C2OCCO2)(C)C

Technology Process of 2-(2,6,6-Trimethylcyclohex-2-en-1-yl)-1,3-dioxolane

There total 2 articles about 2-(2,6,6-Trimethylcyclohex-2-en-1-yl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.5%

: 432-25-7
2,6,6-trimethylcyclohex-1-enecarbaldehyde

: 107-21-1
ethylene glycol

: 78842-55-4
2-[1,3]dioxolan-2-yl-1,3,3-trimethyl-cyclohexene

: 78842-54-3
α-cyclocitral ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 13h; Title compound not separated from byproducts; Heating;

Reference yield:

: 14505-74-9,41721-03-3,59462-59-8,432-24-6
α-cyclocitral

: 78842-54-3
α-cyclocitral ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: Rexyn 201 (OH form) / methanol

2: 62.5 percent / p-toluenesulfonic acid / benzene / 13 h / Heating

With Rexyn 201 (OH form); toluene-4-sulfonic acid; In methanol; benzene;