2-Hexenoic acid, 6-cyclohexyl-6-oxo-, methyl ester, (2E)-

Base Information

Chemical Name:2-Hexenoic acid, 6-cyclohexyl-6-oxo-, methyl ester, (2E)-
CAS No.:793669-86-0
Molecular Formula:C₁₃H₂₀O₃
Molecular Weight:224.3
Hs Code.:

Synonyms:

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Chemical Property of 2-Hexenoic acid, 6-cyclohexyl-6-oxo-, methyl ester, (2E)-

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Technology Process of 2-Hexenoic acid, 6-cyclohexyl-6-oxo-, methyl ester, (2E)-

There total 2 articles about 2-Hexenoic acid, 6-cyclohexyl-6-oxo-, methyl ester, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107841-10-1
1-cyclohexyl-4-hydroxybutan-1-one

: 793669-86-0
methyl (E)-6-cyclohexyl-6-oxohex-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: DMSO; (COCl)2; Et₃N / CH₂Cl₂ / -78 °C

2: 171 mg / CH₂Cl₂ / 20 °C

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; 1: Swern oxidation / 2: Wittig reaction;
DOI:10.1016/j.bmc.2004.04.051

Reference yield:

: 66662-25-7
4-cyclohexyl-4-oxobutanal

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 793669-86-0
methyl (E)-6-cyclohexyl-6-oxohex-2-enoate

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2004.04.051

Reference yield:

: 67-56-1
methanol

: 793669-86-0
methyl (E)-6-cyclohexyl-6-oxohex-2-enoate

: methyl 2-(3-cyclohexyl-3-methoxy-1,2-dioxan-6-yl)acetate

: methyl 2-(3-cyclohexyl-3-methoxy-1,2-dioxan-6-yl)acetate

Guidance literature:: methanol; methyl (E)-6-cyclohexyl-6-oxohex-2-enoate; With dihydrogen peroxide; urea; scandium tris(trifluoromethanesulfonate); at 20 ℃; for 48h;

With 2,2,2-trifluoroethanol; diethylamine; at 20 ℃; for 8h; Title compound not separated from byproducts;
DOI:10.1016/j.bmc.2004.04.051