2-Butenoic acid, 3-amino-4-methoxy-, ethyl ester

Base Information

• Chemical Name: 2-Butenoic acid, 3-amino-4-methoxy-, ethyl ester
• CAS No.: 79534-96-6
• Molecular Formula: C₇H₁₃NO₃
• Molecular Weight: 159.185
• Mol file: 79534-96-6.mol

Synonyms:2-Butenoic acid,3-amino-4-methoxy-,ethyl ester;ethyl 3-amino-4-methoxycrotonate;

Chemical Property of 2-Butenoic acid, 3-amino-4-methoxy-, ethyl ester

Chemical Property:

• PSA: 61.55000
• LogP: 0.73880

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Butenoic acid, 3-amino-4-methoxy-, ethyl ester

There total 1 articles about 2-Butenoic acid, 3-amino-4-methoxy-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 4-methoxy-3-oxobutanoate (66762-68-3) → γ-methoxy-β-aminocrotonic acid ethyl ester (79534-96-6)

Guidance literature:

With ammonia; In ethanol;

DOI:10.1016/0223-5234(91)90132-7

Reference yield: 8.0%

2-chloro-benzaldehyde (89-98-5) + γ-methoxy-β-aminocrotonic acid ethyl ester (79534-96-6) + ethyl 4-[2-(phthalimido)ethoxy]acetoacetate (88150-75-8) → 4-(2-Chloro-phenyl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethoxymethyl]-6-methoxymethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester (140171-55-7)

Guidance literature:

Heating;

DOI:10.1016/0223-5234(91)90132-7

Reference yield:

3-ethoxycarbonyl-2-oxopropionaldehyde (600160-23-4) + 3-nitro-benzaldehyde (99-61-6) + γ-methoxy-β-aminocrotonic acid ethyl ester (79534-96-6) → 2-methoxymethyl-4-(3'-nitrophenyl)-1,4-dihydropyridine-3,5,6-tricarboxylic acid triethyl ester (55551-60-5)

Guidance literature:

In ethanol;

upstream raw materials:

ethyl 4-methoxy-3-oxobutanoate

Downstream raw materials:

4-(2-Chloro-phenyl)-2-[2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-ethoxymethyl]-6-methoxymethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

2-(2-Amino-ethoxymethyl)-4-(2-chloro-phenyl)-6-methoxymethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

6-(4-chlorophenyl)-5-(2,4-dichlorophenyl)-2-methoxymethylpyridine-3-carboxylic acid ethyl ester

2-methoxymethyl-4-(3'-nitrophenyl)-1,4-dihydropyridine-3,5,6-tricarboxylic acid triethyl ester

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