N-Methylhydrazinecarboximidamide hydroiodide

Base Information

• Chemical Name: N-Methylhydrazinecarboximidamide hydroiodide
• CAS No.: 33398-79-7
• Molecular Formula: C₂H₈N₄*HI
• Molecular Weight: 216.025
• Hs Code.: 2928000090
• European Community (EC) Number: 823-538-5
• NSC Number: 72518
• DSSTox Substance ID: DTXSID30381713
• Mol file: 33398-79-7.mol

Synonyms:N-Methylhydrazinecarboximidamide hydroiodide;33398-79-7;1-amino-2-methylguanidine;hydroiodide;1-Amino-3-methylguanidine hydroiodide;N-METHYLHYDRAZINECARBOXIMIDAMIDEHYDROIODIDE;N1-METHYLHYDRAZINE-1-CARBOXIMIDAMIDE HYDROIODIDE;SCHEMBL10971627;DTXSID30381713;APGVZAAHWBJTFZ-UHFFFAOYSA-N;NSC72518;MFCD00179313;NSC-72518;AKOS025116921;N'-amino-N-methylguanidine hydroiodide;N-amino-N'-methylguanidine hydroiodide;AT32122;BS-28014;CS-0371525;EN300-124471;N'-Methyl-1-hydrazinecarboximidamide hydriodide;N'-Methylhydrazinecarboximidamide--hydrogen iodide (1/1);Z2301534051

Chemical Property of N-Methylhydrazinecarboximidamide hydroiodide

Chemical Property:

• Boiling Point: 197°Cat760mmHg
• Flash Point: 72.9°C
• PSA: 73.93000
• Density: 1.33g/cm³
• LogP: 1.18390
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 215.98719
• Heavy Atom Count: 7
• Complexity: 56.6

Purity/Quality:

99%, ^*data from raw suppliers

1-Methyl-3-aminoguanidineHydriodide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN=C(N)NN.I
• Uses: 1-Methyl-3-aminoguanidine Hydriodide is a useful reactant for preparing heterocyclic aldehydes.

Technology Process of N-Methylhydrazinecarboximidamide hydroiodide

There total 5 articles about N-Methylhydrazinecarboximidamide hydroiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

thiosemicarbazide (79-19-6) + methylamine (74-89-5) → N-methylhydrazinecarboximidamide hydroiodide (33398-79-7)

Guidance literature:

thiosemicarbazide; With methyl iodide; In methanol; at 60 ℃; for 1h;

methylamine; In methanol; at 60 - 70 ℃;

Reference yield:

→ N-methylhydrazinecarboximidamide hydroiodide (33398-79-7)

Guidance literature:

With water; hydrazine hydrate;

DOI:10.1021/ja01296a036

Reference yield:

S-methylisothiosemicarbazide hydriodide (35600-34-1) + methylamine (74-89-5) → N-methylhydrazinecarboximidamide hydroiodide (33398-79-7)

Guidance literature:

With water;

DOI:10.1021/ja01296a036

upstream raw materials:

S-methylisothiosemicarbazide hydriodide

methylamine

S-methyl isothiosemicarbazide hydroiodide

thiosemicarbazide

Downstream raw materials:

C₁₇H₁₉N₆⁽¹⁺⁾*2Br^(1-)*H⁽¹⁺⁾

C₁₅H₁₇N₆S⁽¹⁺⁾*HI*I^(1-)

C₁₇H₁₈N₇O₂⁽¹⁺⁾*2Br^(1-)*H⁽¹⁺⁾

Brenztraubensaeure-N-methyl-guanylhydrazon