L-Phenylalanine, hexyl ester

Base Information

• Chemical Name: L-Phenylalanine, hexyl ester
• CAS No.: 81686-34-2
• Molecular Formula: C15H23NO2
• Molecular Weight: 249.353
• Mol file: 81686-34-2.mol

Synonyms:

Chemical Property of L-Phenylalanine, hexyl ester

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of L-Phenylalanine, hexyl ester

There total 1 articles about L-Phenylalanine, hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

L-phenylalanine (63-91-2,25191-15-5,658-69-5,67675-33-6) + hexan-1-ol (111-27-3) → L-Phenylalanine hexyl ester (81686-34-2)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 12h; Reflux; Dean-Stark; Green chemistry;

DOI:10.1039/c9gc00030e

Reference yield: 97.0%

L-Phenylalanine hexyl ester (81686-34-2) + 2-Bromoacetyl bromide (598-21-0) → hexyl (2-bromoacetyl)-L-phenylalaninate

Guidance literature:

With sodium carbonate; In dichloromethane; at 20 ℃; for 12h; Green chemistry;

DOI:10.1039/c9gc00030e

Reference yield: 54.0%

oxalyl dichloride (79-37-8) + L-Phenylalanine hexyl ester (81686-34-2) → dihexyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate (500906-12-7)

Guidance literature:

With triethylamine; In dichloromethane; for 24h;

DOI:10.1016/S0957-4166(02)00506-2

upstream raw materials:

L-phenylalanine

hexan-1-ol

Downstream raw materials:

dihexyl (2S,7S)-3,6-diaza-4,5-dioxo-2,7-dibenzyloctano-1,8-dicarboxylate