Methanetetramine, octamethyl-

Base Information

Chemical Name:Methanetetramine, octamethyl-
CAS No.:10524-51-3
Molecular Formula:C9H24 N4
Molecular Weight:188.316
Hs Code.:
DSSTox Substance ID:DTXSID60147026
Nikkaji Number:J795.253H
Wikidata:Q83011931
Mol file:10524-51-3.mol

Synonyms:Methanetetramine, octamethyl-;10524-51-3;N,N,N',N',N'',N'',N''',N'''-Octamethylmethanetetraamine;Tetrakis(dimethylamino)methane;tetrakis(dimethylamino) methane;SCHEMBL2567749;DTXSID60147026;dimethyl-[tris(dimethylamino)-methyl]-amine

Suppliers and Price of Methanetetramine, octamethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanetetramine, octamethyl-

Chemical Property:

Boiling Point:219.7°Cat760mmHg
Flash Point:75.4°C
Density:0.913g/cm³
XLogP3:0.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:188.20009678
Heavy Atom Count:13
Complexity:114

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C(N(C)C)(N(C)C)N(C)C

Technology Process of Methanetetramine, octamethyl-

There total 1 articles about Methanetetramine, octamethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 30388-20-6
N,N,N',N',N'',N''-hexamethylguanidinium chloride

: 124-40-3
dimethyl amine

: 5762-56-1
tris(dimethylamino)methane

: 10524-51-3
Tetrakis(dimethylamino)methan

Guidance literature:: dimethyl amine; With Trimethyl borate; sodium hydride; In tetrahydrofuran; for 0.25h; cooling;

N,N,N',N',N'',N''-hexamethylguanidinium chloride; In tetrahydrofuran; at 20 ℃; for 48h;

Reference yield: 80.0%

: 10524-51-3
Tetrakis(dimethylamino)methan

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: {C(N(CH₃)2)3}⁽¹⁺⁾*{(CO)3NiC(O)N(CH₃)2}^(1-)={C(N(CH₃)2)3}{(CO)3NiC(O)N(CH₃)2}

Guidance literature:: In benzene; prepn. from C(N(CH3)2)4 and Ni(CO)4 in benzene at 5 °C (several days);;
DOI:10.1016/S0022-328X(00)92115-6

Reference yield: 70.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 10524-51-3
Tetrakis(dimethylamino)methan

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: {C(N(CH₃)2)3}⁽¹⁺⁾*{(CO)3NiC(O)N(CH₃)2}^(1-)={C(N(CH₃)2)3}{(CO)3NiC(O)N(CH₃)2}

: 2((CH₃)2N)3C⁽¹⁺⁾*Ni₅(CO)12^(2-)*C₄H₈O=[((CH₃)2N)3C]2[Ni₅(CO)12]*C₄H₈O

: 3((CH₃)2N)3C⁽¹⁺⁾*Ni₆(CO)12^(2-)*O₂CN(CH₃)2^(1-)=[((CH₃)2N)3C]3[Ni₆(CO)12][O₂CN(CH₃)2]

Guidance literature:: In tetrahydrofuran; under Ar, 1 equiv. of Ni-compd. was added to C(NMe2)4 soln. in THF at 0 °C; at room temp. mainly ((Me2N)3C)2Ni5(CO)12*THF was formed; filtn., n-pentane was added, ((Me2N)3C)2Ni5(CO)12*THF was filtered off, n-pentane addn./crystn. for several days, ((Me2N)3C)3Ni6(CO)12O2CNMe2 was filtered off, n-pentane was added at 0 °C, crystals was sepd and oil was dried in vac., elem. anal.;
DOI:10.1002/1521-3749(200109)627:9<2274::aid-zaac2274>3.0.co;2-9