Butanoic acid, 2,4-bis[[(1,1-dimethylethoxy)carbonyl]amino]-, pentafluorophenyl ester, (2S)-

Base Information

Chemical Name:Butanoic acid, 2,4-bis[[(1,1-dimethylethoxy)carbonyl]amino]-, pentafluorophenyl ester, (2S)-
CAS No.:817562-97-3
Molecular Formula:C20H25F5N2O6
Molecular Weight:484.42
Hs Code.:

Synonyms:Boc-Dab(Boc)-OPfp;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Butanoic acid, 2,4-bis[[(1,1-dimethylethoxy)carbonyl]amino]-, pentafluorophenyl ester, (2S)-

Chemical Property:

PSA：102.96000
LogP:4.87740

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Butanoic acid, 2,4-bis[[(1,1-dimethylethoxy)carbonyl]amino]-, pentafluorophenyl ester, (2S)-

There total 2 articles about Butanoic acid, 2,4-bis[[(1,1-dimethylethoxy)carbonyl]amino]-, pentafluorophenyl ester, (2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 201472-66-4
dicyclohexylamine salt of (2S)-2,4-bis[(tert-butoxycarbonyl)amino]butanoic acid

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 817562-97-3
2,4-di[(tert-butoxycarbonyl)amino]butyric acid pentafluorophenyl ester

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/ja800834y

Reference yield:

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 817562-97-3
2,4-di[(tert-butoxycarbonyl)amino]butyric acid pentafluorophenyl ester

Guidance literature:: dicyclohexylamine salt of (2S)-2,4-bis[(tert-butoxycarbonyl)amino]butanoic acid; With potassium hydrogensulfate; In dichloromethane; water; at 22 - 25 ℃; for 1h;

2,3,4,5,6-pentafluorophenol; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 22 - 25 ℃; for 2h;