1,3-Benzenedicarboxylic acid, 5-hydroxy-4-(2-hydroxybenzoyl)-

Base Information

Chemical Name:1,3-Benzenedicarboxylic acid, 5-hydroxy-4-(2-hydroxybenzoyl)-
CAS No.:820243-51-4
Molecular Formula:C15H10O7
Molecular Weight:302.24
Hs Code.:
DSSTox Substance ID:DTXSID40458869
Nikkaji Number:J2.131.159F
Wikidata:Q82282418

Synonyms:820243-51-4;1,3-Benzenedicarboxylic acid, 5-hydroxy-4-(2-hydroxybenzoyl)-;SCHEMBL22938974;DTXSID40458869;4-(2-Hydroxybenzoyl)-5-hydroxyisophthalic acid

Suppliers and Price of 1,3-Benzenedicarboxylic acid, 5-hydroxy-4-(2-hydroxybenzoyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,3-Benzenedicarboxylic acid, 5-hydroxy-4-(2-hydroxybenzoyl)-

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:302.04265265
Heavy Atom Count:22
Complexity:461

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)C2=C(C=C(C=C2O)C(=O)O)C(=O)O)O

Technology Process of 1,3-Benzenedicarboxylic acid, 5-hydroxy-4-(2-hydroxybenzoyl)-

There total 4 articles about 1,3-Benzenedicarboxylic acid, 5-hydroxy-4-(2-hydroxybenzoyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026688-54-9
5-benzyloxy-4-(2-benzyloxy-benzoyl)-isophthalic acid

: 820243-51-4
5-hydroxy-4-(2-hydroxybenzoyl)isophthalic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 12h; under 750.06 Torr;
DOI:10.1021/jo049228l

Reference yield:

: 820243-52-5
(2,4-dibromo-6-hydroxyphenyl)-(2-hydroxyphenyl)methanone

: 820243-51-4
5-hydroxy-4-(2-hydroxybenzoyl)isophthalic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / K₂CO₃ / dimethylformamide / 12 h / 80 °C

2: 92 percent / Et₃N; (dppf)PdCl₂; dppf / dimethylformamide / 18 h / 80 °C / 750.06 Torr

3: KOH / methanol / 48 h / 60 °C

4: 414 mg / H₂ / Pd/C / ethanol / 12 h / 20 °C / 750.06 Torr

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium hydroxide; hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo049228l

Reference yield:

: 820243-55-8
5-benzyloxy-4-(2-benzyloxybenzoyl)isophthalic acid dimethyl ester

: 820243-51-4
5-hydroxy-4-(2-hydroxybenzoyl)isophthalic acid

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / methanol / 48 h / 60 °C

2: 414 mg / H₂ / Pd/C / ethanol / 12 h / 20 °C / 750.06 Torr

With potassium hydroxide; hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jo049228l