2-Cyclohexene-1-carbonitrile, 1-[(trimethylsilyl)oxy]-

Base Information

Chemical Name:2-Cyclohexene-1-carbonitrile, 1-[(trimethylsilyl)oxy]-
CAS No.:82053-13-2
Molecular Formula:C10H17NOSi
Molecular Weight:195.337
Hs Code.:
DSSTox Substance ID:DTXSID50453421
Nikkaji Number:J1.067.549I

Synonyms:2-Cyclohexene-1-carbonitrile, 1-[(trimethylsilyl)oxy]-;SCHEMBL10887357;DTXSID50453421;82053-13-2;3-(Trimethylsiloxy)cyclohexene-3-carbonitrile

Suppliers and Price of 2-Cyclohexene-1-carbonitrile, 1-[(trimethylsilyl)oxy]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Cyclohexene-1-carbonitrile, 1-[(trimethylsilyl)oxy]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:195.107940700
Heavy Atom Count:13
Complexity:258

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)OC1(CCCC=C1)C#N

Technology Process of 2-Cyclohexene-1-carbonitrile, 1-[(trimethylsilyl)oxy]-

There total 6 articles about 2-Cyclohexene-1-carbonitrile, 1-[(trimethylsilyl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 930-68-7
cyclohexenone

: 7677-24-9
trimethylsilyl cyanide

: 82053-13-2
1-trimethylsiloxy-2-cyclohexene-1-carbonitrile

Guidance literature:: With P(i-PrNCH₂CH₂)N; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1016/j.tetlet.2005.09.032

Reference yield: 88.0%

: 930-68-7
cyclohexenone

: 7677-24-9
trimethylsilyl cyanide

: 82053-13-2
1-trimethylsiloxy-2-cyclohexene-1-carbonitrile

: 1-hydroxycyclohex-2-enecarbonitrile

Guidance literature:: With trimethylsilyl bis(trifluoromethanesulfonyl)imide; In dichloromethane; at -78 ℃; for 0.75h;
DOI:10.1080/00397919608003546

Reference yield: 49.0%

: 930-68-7
cyclohexenone

: 7677-24-9
trimethylsilyl cyanide

: 66885-88-9
3-trimethylsiloxy-2-cyclohexene-1-carbonitrile

: 82053-13-2
1-trimethylsiloxy-2-cyclohexene-1-carbonitrile

: 136583-99-8
1-trimethylsiloxy-1,3-cyclohexanedicarbonitrile

Guidance literature:: With hydroxyapatite; In toluene; at 0 ℃; for 5h; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1246/bcsj.66.2016