Pentane, 1,1-dichloro-

Base Information

• Chemical Name: Pentane, 1,1-dichloro-
• CAS No.: 820-55-3
• Molecular Formula: C5H10Cl2
• Molecular Weight: 141.04
• Mol file: 820-55-3.mol

Synonyms:

Chemical Property of Pentane, 1,1-dichloro-

Chemical Property:

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Pentane, 1,1-dichloro-

There total 3 articles about Pentane, 1,1-dichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pentane (109-66-0,8031-35-4,9078-70-0) → 1-Chloropentane (543-59-9) + 1,1-dichloropentane (820-55-3)

Guidance literature:

With nitrosylchloride; at 350 ℃;

Reference yield:

1-Chloropentane (543-59-9) → 1,2-dichloropentane (1674-33-5) + 1,4-dichloropentane (626-92-6) + 1,3-dichloro-pentane (30122-12-4,140237-88-3,140237-89-4) + 1,1-dichloropentane (820-55-3) + 1,5-dichloropentane (628-76-2)

Guidance literature:

With N-chloropiperidine; 2,2'-azobis(isobutyronitrile); In trifluoroacetic acid; at 30 ℃; Product distribution; Rate constant; Irradiation; relative rate constants, position selectivity, substrate selectivity;

Reference yield:

tetrachloromethane (56-23-5) + caprophenone (942-92-7) → 1,1-dichloropentane (820-55-3) + benzoic acid (65-85-0,8013-63-6) + 2-phenyl-2-(trichloromethyl)-3-n-butyloxirane (97295-24-4)

Guidance literature:

With sodium hydroxide; tetrabutylammomium bromide; for 7h; Ambient temperature;

DOI:10.1021/jo00220a010

upstream raw materials:

pentane

tetrachloromethane

caprophenone

1-Chloropentane

Downstream raw materials:

octachlorocyclopentene

maleic acid

2,2-dichlorohexanal

1-Chloropentane

Refernces

• 1、 Dneprovskii, A. S.,Mil'tsov, S. A.,Arbuzov, P. V.. "MECHANISMS OF FREE-RADICAL REACTIONS. XXIV. QUANTITATIVE DESCRIPTION OF THE POLAR EFFECTS OF SUBSTITUENTS ON THE KINETICS OF THE FREE-RADICAL CHLORINATION OF ALIPHATIC COMPOUNDS BY N-CHLOROPIPERIDINE". . p. 1826 - 1835. Retrieved 2007/10/02.
• 2、 Dneprovskii, A. S.,Mil'tsov, S. A.. "MECHANISMS OF FREE-RADICAL REACTIONS. XIX. SELECTIVITY OF THE FREE-RADICAL CHLORINATION OF 1-CHLOROALKANES BY N-CHLOROPIPERIDINE". . p. 265 - 269. Retrieved 2007/10/02.