[1-(Cyclohex-1-en-1-yl)cyclopropyl](trimethyl)silane

Base Information

Chemical Name:[1-(Cyclohex-1-en-1-yl)cyclopropyl](trimethyl)silane
CAS No.:82084-04-6
Molecular Formula:C12H22Si
Molecular Weight:194.392
Hs Code.:
DSSTox Substance ID:DTXSID60511809
Wikidata:Q82370785

Synonyms:82084-04-6;[1-(Cyclohex-1-en-1-yl)cyclopropyl](trimethyl)silane;DTXSID60511809;[1-(1-cyclohexen-1-yl)cyclopropyl](trimethyl)silane

Suppliers and Price of [1-(Cyclohex-1-en-1-yl)cyclopropyl](trimethyl)silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of [1-(Cyclohex-1-en-1-yl)cyclopropyl](trimethyl)silane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:194.149077236
Heavy Atom Count:13
Complexity:228

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C1(CC1)C2=CCCCC2

Technology Process of [1-(Cyclohex-1-en-1-yl)cyclopropyl](trimethyl)silane

There total 6 articles about [1-(Cyclohex-1-en-1-yl)cyclopropyl](trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82195-54-8
1-(1-trimethylsilylcyclopropyl)cyclohexanol

: 82084-04-6
L-(1-trimethylsilylcyclopropyl)cyclohexene

Guidance literature:: With toluene-4-sulfonic acid; In benzene; at 20 ℃; Yield given;
DOI:10.1016/S0040-4039(00)86803-3

Reference yield:

: 51666-97-8
1-<α-(trimethylsilyl)vinyl>cyclohexan-1-ol

: 82084-04-6
L-(1-trimethylsilylcyclopropyl)cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) EtZnI / 1.) ether, 1 h, reflux, 2.) 0 deg C, ether

2: silica gel / hexane

With silica gel; ethylzinc iodide; In hexane;
DOI:10.1016/S0040-4020(01)88590-2

Reference yield:

: 31469-29-1
(1'-(trimethylsilyl)cyclopropyl)carboxylic acid

: 82084-04-6
L-(1-trimethylsilylcyclopropyl)cyclohexene

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / red mercuric oxide, Br₂ / CH₂Cl₂ / 2 h

2: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 3 h

3: silica gel / hexane

With n-butyllithium; bromine; silica gel; mercury(II) oxide; In hexane; dichloromethane;
DOI:10.1016/S0040-4020(01)88590-2