N,N-diethyldecan-1-amine

Base Information

• Chemical Name: N,N-diethyldecan-1-amine
• CAS No.: 6308-94-7
• Molecular Formula: C14H31 N
• Molecular Weight: 213.407
• Hs Code.: 2921199090
• Mol file: 6308-94-7.mol

Synonyms:Decylamine,N,N-diethyl- (8CI); N,N-Diethyl-1-decanamine; NSC 41196; NSC 41720

Chemical Property of N,N-diethyldecan-1-amine

Chemical Property:

• Vapor Pressure: 0.014mmHg at 25°C
• Melting Point: -20.3°C (estimate)
• Refractive Index: 1.4357
• Boiling Point: 258.1°C at 760 mmHg
• PKA: 10.59±0.25(Predicted)
• Flash Point: 99.7°C
• PSA: 3.24000
• Density: 0.799g/cm³
• LogP: 4.46890

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-diethyldecan-1-amine

There total 6 articles about N,N-diethyldecan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ethanol (64-17-5) + 1-Decanol (112-30-1) + acetonitrile (75-05-8,26809-02-9) → n-decyldiethylamine (6308-94-7) + triethylamine (121-44-8)

Guidance literature:

With hydrogen; copper; at 240 ℃; under 7600 Torr;

Reference yield:

N,N-diethyldecanamide (2602-61-1) → 1-Decanol (112-30-1) + n-decyldiethylamine (6308-94-7)

Guidance literature:

With sodium (tert-butylamino)trihydroborate; In tetrahydrofuran; at 66 ℃; for 96h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; further reducing agent: sodium (dimethylamino)trihydroborat (NaDMAB);

DOI:10.1021/jo00187a028

Reference yield:

caprinaldehyde (112-31-2) + diethylamine (109-89-7) → 1-Decanol (112-30-1) + n-decyldiethylamine (6308-94-7) + N,N-diethyldecylenamine

Guidance literature:

With acetylacetonato(1,5-cyclooctadiene)rhodium(I); hydrogen; triphenylphosphine; In dodecane; N,N-dimethyl-formamide; at 100 ℃; for 1h; under 15001.5 Torr; Autoclave;

DOI:10.1021/acs.oprd.9b00409

upstream raw materials:

N,N-diethyldecanamide

ethanol

1-Decanol

acetonitrile

Refernces

• 1、 Kozlov,Tereshko,Basalaeva,Tarasevich. "Joint Synthesis of Tertiary Unsymmetrical and Symmetrical Aliphatic Amines". . p. 1095 - 1098. Retrieved 2007/10/03.