Benzamide, 2-amino-N-(2-iodophenyl)-N-methyl-

Base Information

Chemical Name:Benzamide, 2-amino-N-(2-iodophenyl)-N-methyl-
CAS No.:826991-71-3
Molecular Formula:C14H13IN2O
Molecular Weight:352.175
Hs Code.:
DSSTox Substance ID:DTXSID70479542
Wikidata:Q82313637

Synonyms:826991-71-3;Benzamide, 2-amino-N-(2-iodophenyl)-N-methyl-;DTXSID70479542

Suppliers and Price of Benzamide, 2-amino-N-(2-iodophenyl)-N-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzamide, 2-amino-N-(2-iodophenyl)-N-methyl-

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:352.00726
Heavy Atom Count:18
Complexity:298

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C1=CC=CC=C1I)C(=O)C2=CC=CC=C2N

Technology Process of Benzamide, 2-amino-N-(2-iodophenyl)-N-methyl-

There total 4 articles about Benzamide, 2-amino-N-(2-iodophenyl)-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 826991-63-3
N-(2-iodo-phenyl)-N-methyl-2-nitro-benzamide

: 826991-71-3
2-amino-N-(2-iodo-phenyl)-N-methyl-benzamide

Guidance literature:: With tin(ll) chloride; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1039/b602912d

Reference yield:

: 34489-87-7
N-(2-iodo-phenyl)-2-nitro-benzamide

: 826991-71-3
2-amino-N-(2-iodo-phenyl)-N-methyl-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / NaH / tetrahydrofuran / 20 °C

2: 100 percent / SnCl₂*H₂O / dimethylformamide / 24 h / 20 °C

With sodium hydride; tin(ll) chloride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b602912d

Reference yield:

: 615-43-0
2-iodophenylamine

: 826991-71-3
2-amino-N-(2-iodo-phenyl)-N-methyl-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine / CH₂Cl₂ / 20 °C

2: 78 percent / NaH / tetrahydrofuran / 20 °C

3: 100 percent / SnCl₂*H₂O / dimethylformamide / 24 h / 20 °C

With pyridine; sodium hydride; tin(ll) chloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b602912d