N-(2-iodophenyl)-2-nitrobenzamide

Base Information

Chemical Name:N-(2-iodophenyl)-2-nitrobenzamide
CAS No.:34489-87-7
Molecular Formula:C13H9IN2O3
Molecular Weight:368.131
Hs Code.:
DSSTox Substance ID:DTXSID60362459
Nikkaji Number:J2.380.798J
Wikidata:Q82145558

Synonyms:N-(2-iodophenyl)-2-nitrobenzamide;34489-87-7;CBMicro_000122;N-(iodophenyl)nitrobenzamide;Oprea1_630744;DTXSID60362459;SMSF0005239;STK051063;AKOS003283454;CB01295;BIM-0000095.P001;SR-01000205901;SR-01000205901-1

Suppliers and Price of N-(2-iodophenyl)-2-nitrobenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-(2-IODOPHENYL)-2-NITROBENZAMIDE 95.00%
5MG
$ 503.91

Total 0 raw suppliers

Chemical Property of N-(2-iodophenyl)-2-nitrobenzamide

Chemical Property:

PSA：78.41000
LogP:4.35890
XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:367.96579
Heavy Atom Count:19
Complexity:345

Purity/Quality:: N-(2-IODOPHENYL)-2-NITROBENZAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)NC2=CC=CC=C2I)[N+](=O)[O-]

Technology Process of N-(2-iodophenyl)-2-nitrobenzamide

There total 3 articles about N-(2-iodophenyl)-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 615-43-0
2-iodophenylamine

: 610-14-0
2-nitrobenzyl chloride

: 34489-87-7
N-(2-iodo-phenyl)-2-nitro-benzamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.1039/b602912d

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 34489-87-7
N-(2-iodo-phenyl)-2-nitro-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / 3 h / 0 - 75 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

2.2: 5 h / 20 °C / Inert atmosphere

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1002/adsc.201600748