11H-DIBENZO(b,e)(1,4)DIAZEPIN-11-ONE, 5,10-DIHYDRO-10-METHYL-

Base Information

Chemical Name:11H-DIBENZO(b,e)(1,4)DIAZEPIN-11-ONE, 5,10-DIHYDRO-10-METHYL-
CAS No.:32047-69-1
Molecular Formula:C14H12 N2 O
Molecular Weight:224.262
Hs Code.:2933990090
DSSTox Substance ID:DTXSID80185864
Nikkaji Number:J42.202I
Wikidata:Q83057004
Mol file:32047-69-1.mol

Synonyms:32047-69-1;BRN 0654203;11H-DIBENZO(b,e)(1,4)DIAZEPIN-11-ONE, 5,10-DIHYDRO-10-METHYL-;10-Methyl-10,11-dihydro-5H-dibenzo[b,e][1,4]diazepin-11-one;10-Methyl-5,10-dihydro-11H-dibenzo(b,e)(1,4)diazepin-11-one;11H-Dibenzo[b,e][1,4]diazepin-11-one, 5,10-dihydro-10-methyl-;5-methyl-11H-benzo[b][1,4]benzodiazepin-6-one;SCHEMBL7982510;DTXSID80185864;NLKSFKLPWZLDGG-UHFFFAOYSA-N;10-methyl-5,10-dihydro-dibenzo[b,e][1,4]diazepin-11-one;LS-60947;10-methyl-11-oxo-10,11-dihydro-5H-dibenzo[b,e][1,4]diazepine;10methyl-11-oxo-10,11-dihydro-5H-dibenzo[b,e][1,4]diazepine;9-methyl-2,9-diazatricyclo[9.4.0.0?,?]pentadeca-1(11),3(8),4,6,12,14-hexaen-10-one

Suppliers and Price of 11H-DIBENZO(b,e)(1,4)DIAZEPIN-11-ONE, 5,10-DIHYDRO-10-METHYL-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 11H-DIBENZO(b,e)(1,4)DIAZEPIN-11-ONE, 5,10-DIHYDRO-10-METHYL-

Chemical Property:

Vapor Pressure:4.12E-07mmHg at 25°C
Boiling Point:415.4°Cat760mmHg
Flash Point:205.1°C
PSA：37.79000
Density:1.196g/cm³
LogP:2.58200
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:224.094963011
Heavy Atom Count:17
Complexity:305

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=CC=CC=C2NC3=CC=CC=C3C1=O

Technology Process of 11H-DIBENZO(b,e)(1,4)DIAZEPIN-11-ONE, 5,10-DIHYDRO-10-METHYL-

There total 15 articles about 11H-DIBENZO(b,e)(1,4)DIAZEPIN-11-ONE, 5,10-DIHYDRO-10-METHYL- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 5814-41-5
5,10-dihydro-11H-dibenzo[b,e][1,4]-diazepin-11-one

: 74-88-4
methyl iodide

: 32047-69-1
10-methyl-5,10-dihydro-dibenzo[b,e][1,4]diazepin-11-one

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 25 ℃; for 14h;

Reference yield: 63.0%

: 826991-71-3
2-amino-N-(2-iodo-phenyl)-N-methyl-benzamide

: 32047-69-1
10-methyl-5,10-dihydro-dibenzo[b,e][1,4]diazepin-11-one

Guidance literature:: With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; In toluene; at 110 ℃; for 24h;
DOI:10.1016/j.tet.2004.10.061