METHYL 5-METHYLBENZOFURAN-2-CARBOXYLATE

Base Information

• Chemical Name: METHYL 5-METHYLBENZOFURAN-2-CARBOXYLATE
• CAS No.: 82788-34-9
• Molecular Formula: C₁₁H₁₀O₃
• Molecular Weight: 190.199
• Hs Code.: 2932999099
• Mol file: 82788-34-9.mol

Synonyms:methyl 5-methyl-2-benzofurancarboxylate;Methyl-5-methyl-benzofuran-2-carboxylate;5-methylbenzofuran-2-carboxylic acid methyl ester;2-Benzofurancarboxylic acid,5-methyl-,methyl ester;5-Methyl-benzofuran-2-carbonsaeure-methylester;

Chemical Property of METHYL 5-METHYLBENZOFURAN-2-CARBOXYLATE

Chemical Property:

• PSA: 39.44000
• LogP: 2.52780
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Methyl5-methylbenzofuran-2-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYL 5-METHYLBENZOFURAN-2-CARBOXYLATE

There total 8 articles about METHYL 5-METHYLBENZOFURAN-2-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 5-methylbenzofuran-2-carboxylic acid (10242-09-8) → methyl 5-methylbenzofuran-2-carboxylate (82788-34-9)

Guidance literature:

In diethyl ether; for 0.333333h; Ambient temperature;

DOI:10.1246/bcsj.56.2762

Reference yield: 42.0%

2-hydroxy-5-methylbenzaldehyde (613-84-3) → methyl 5-methylbenzofuran-2-carboxylate (82788-34-9)

Guidance literature:

With Bu₄NBr; potassium carbonate; In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; toluene;

Reference yield: 42.0%

→ methyl 5-methylbenzofuran-2-carboxylate (82788-34-9)

Guidance literature:

upstream raw materials:

methanol

5-methylbenzofuran-2-carboxylic acid

diazomethane

methyl 5-nitrofuran-2-carboxylate

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