3-Chloro-3-phenoxy-3H-diazirine

Base Information

Chemical Name:3-Chloro-3-phenoxy-3H-diazirine
CAS No.:82849-43-2
Molecular Formula:C7H5ClN2O
Molecular Weight:168.583
Hs Code.:
DSSTox Substance ID:DTXSID20518450
Nikkaji Number:J2.512.077I

Synonyms:3-Chloro-3-phenoxy-3H-diazirine;82849-43-2;DTXSID20518450;3-Chloro-3-phenoxy-3H-diazirene

Suppliers and Price of 3-Chloro-3-phenoxy-3H-diazirine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-Chloro-3-phenoxy-3H-diazirine

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:168.0090405
Heavy Atom Count:11
Complexity:171

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)OC2(N=N2)Cl

Technology Process of 3-Chloro-3-phenoxy-3H-diazirine

There total 6 articles about 3-Chloro-3-phenoxy-3H-diazirine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 651306-32-0
N-(methanesulfonyloxy)-O-phenylisourea

: 82849-43-2
3-chloro-3-phenoxy-3H-diazirine

Guidance literature:: With sodium hypochlorite; lithium chloride; In methanol; water; at 0 ℃; for 0.5h;
DOI:10.1021/ol701804m

Reference yield: 37.0%

: 3170-96-5
N-(benzenesulfonyloxy)-O-phenylisourea

: 82849-43-2
3-chloro-3-phenoxy-3H-diazirine

Guidance literature:: With sodium hypochlorite; dimethyl sulfoxide; lithium chloride; sodium chloride; In pentane; at -5 ℃; for 0.833333h;
DOI:10.1021/jo00143a001

Reference yield:

: 3174-90-1
N-hydroxyl-O-phenylisourea

: 82849-43-2
3-chloro-3-phenoxy-3H-diazirine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 4 h / 20 °C

2: 50 percent / LiCl; qa. sodium hypochlorite; NaCl / dimethylsulfoxide; pentane / cooling

With pyridine; sodium hypochlorite; lithium chloride; sodium chloride; In dichloromethane; dimethyl sulfoxide; pentane;
DOI:10.1021/ja050103n