1,2-Pyrrolidinedicarboxylic acid, 4-hydroxy-, 1-[2,2-dimethoxy-2-(3,4,5-trimethoxyphenyl)ethyl] 2-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl] ester, (2S,4R)-

Base Information

Chemical Name:1,2-Pyrrolidinedicarboxylic acid, 4-hydroxy-, 1-[2,2-dimethoxy-2-(3,4,5-trimethoxyphenyl)ethyl] 2-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl] ester, (2S,4R)-
CAS No.:828921-10-4
Molecular Formula:C30H39NO14
Molecular Weight:637.638
Hs Code.:

1,2-Pyrrolidinedicarboxylic acid, 4-hydroxy-,
1-[2,2-dimethoxy-2-(3,4,5-trimethoxyphenyl)ethyl]
2-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl] ester, (2S,4R)-

Synonyms:

Suppliers and Price of 1,2-Pyrrolidinedicarboxylic acid, 4-hydroxy-, 1-[2,2-dimethoxy-2-(3,4,5-trimethoxyphenyl)ethyl] 2-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl] ester, (2S,4R)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Pyrrolidinedicarboxylic acid, 4-hydroxy-, 1-[2,2-dimethoxy-2-(3,4,5-trimethoxyphenyl)ethyl] 2-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl] ester, (2S,4R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,2-Pyrrolidinedicarboxylic acid, 4-hydroxy-, 1-[2,2-dimethoxy-2-(3,4,5-trimethoxyphenyl)ethyl] 2-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl] ester, (2S,4R)-

There total 3 articles about 1,2-Pyrrolidinedicarboxylic acid, 4-hydroxy-, 1-[2,2-dimethoxy-2-(3,4,5-trimethoxyphenyl)ethyl] 2-[2-oxo-2-(3,4,5-trimethoxyphenyl)ethyl] ester, (2S,4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51490-01-8
1-(3,4,5-trimethoxyphenyl)-2-bromoethanone

: (2S,4R)-4-Hydroxy-pyrrolidine-1,2-dicarboxylic acid 1-[2,2-dimethoxy-2-(3,4,5-trimethoxy-phenyl)-ethyl] ester

: 828921-10-4
(2S,4R)-4-Hydroxy-pyrrolidine-1,2-dicarboxylic acid 1-[2,2-dimethoxy-2-(3,4,5-trimethoxy-phenyl)-ethyl] ester 2-[2-oxo-2-(3,4,5-trimethoxy-phenyl)-ethyl] ester

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.416667h;
DOI:10.1021/ja044702q

Reference yield:

: 1136-86-3
methyl (3,4,5-trimethoxyphenyl) ketone

: 828921-10-4
(2S,4R)-4-Hydroxy-pyrrolidine-1,2-dicarboxylic acid 1-[2,2-dimethoxy-2-(3,4,5-trimethoxy-phenyl)-ethyl] ester 2-[2-oxo-2-(3,4,5-trimethoxy-phenyl)-ethyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / KOH; iodobenzene diacetate / 18 h / 20 °C

2: TEA / tetrahydrofuran; toluene / 1.33 h / 0 - 20 °C

3: aq. Na₂CO₃ / tetrahydrofuran / 0 - 20 °C

4: 1.90 g / Cs₂CO₃ / dimethylformamide / 0.42 h / 0 - 20 °C

With potassium hydroxide; [bis(acetoxy)iodo]benzene; TEA; sodium carbonate; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja044702q

Reference yield:

: 828921-08-0
2,2-dimethoxy-2-(3,4,5-trimethoxy-phenyl)-ethanol

: 828921-10-4
(2S,4R)-4-Hydroxy-pyrrolidine-1,2-dicarboxylic acid 1-[2,2-dimethoxy-2-(3,4,5-trimethoxy-phenyl)-ethyl] ester 2-[2-oxo-2-(3,4,5-trimethoxy-phenyl)-ethyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: TEA / tetrahydrofuran; toluene / 1.33 h / 0 - 20 °C

2: aq. Na₂CO₃ / tetrahydrofuran / 0 - 20 °C

3: 1.90 g / Cs₂CO₃ / dimethylformamide / 0.42 h / 0 - 20 °C

With TEA; sodium carbonate; caesium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja044702q