Benzamide, 4-chloro-N-methyl-N-(2-thienylmethyl)-

Base Information

Chemical Name:Benzamide, 4-chloro-N-methyl-N-(2-thienylmethyl)-
CAS No.:830330-68-2
Molecular Formula:C13H12ClNOS
Molecular Weight:265.763
Hs Code.:
DSSTox Substance ID:DTXSID00458062
Wikidata:Q82281193

Synonyms:830330-68-2;Benzamide, 4-chloro-N-methyl-N-(2-thienylmethyl)-;DTXSID00458062

Suppliers and Price of Benzamide, 4-chloro-N-methyl-N-(2-thienylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzamide, 4-chloro-N-methyl-N-(2-thienylmethyl)-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:265.0328129
Heavy Atom Count:17
Complexity:266

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(CC1=CC=CS1)C(=O)C2=CC=C(C=C2)Cl

Technology Process of Benzamide, 4-chloro-N-methyl-N-(2-thienylmethyl)-

There total 3 articles about Benzamide, 4-chloro-N-methyl-N-(2-thienylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 74-88-4
methyl iodide

: 332082-86-7
4-Chloro-N-thiophen-2-ylmethyl-benzamide

: 830330-68-2
4-chloro-N-methyl-N-thiophen-2-ylmethylbenzamide

Guidance literature:: 4-Chloro-N-thiophen-2-ylmethyl-benzamide; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;

methyl iodide; In tetrahydrofuran; for 1h;
DOI:10.1021/jm031112e

Reference yield:

: 27757-85-3
2-Aminomethylthiophene

: 830330-68-2
4-chloro-N-methyl-N-thiophen-2-ylmethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / iPr₂NEt / CH₂Cl₂ / 0 - 20 °C

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 98 percent / tetrahydrofuran / 1 h

With sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm031112e

Reference yield:

: 122-01-0
4-chloro-benzoyl chloride

: 830330-68-2
4-chloro-N-methyl-N-thiophen-2-ylmethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / iPr₂NEt / CH₂Cl₂ / 0 - 20 °C

2.1: NaH / tetrahydrofuran / 0 - 20 °C

2.2: 98 percent / tetrahydrofuran / 1 h

With sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm031112e