2-[2-(2-Sulfanylphenyl)sulfanylethylsulfanyl]benzenethiol

Base Information

Chemical Name:2-[2-(2-Sulfanylphenyl)sulfanylethylsulfanyl]benzenethiol
CAS No.:83209-89-6
Molecular Formula:C14H14S4
Molecular Weight:310.529
Hs Code.:
DSSTox Substance ID:DTXSID20565146
Nikkaji Number:J897.940E
Wikidata:Q82450096

Synonyms:83209-89-6;DTXSID20565146;2,2'-(Ethane-1,2-diyldisulfanediyl)di(benzene-1-thiol)

Suppliers and Price of 2-[2-(2-Sulfanylphenyl)sulfanylethylsulfanyl]benzenethiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-[2-(2-Sulfanylphenyl)sulfanylethylsulfanyl]benzenethiol

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:309.99783514
Heavy Atom Count:18
Complexity:210

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)S)SCCSC2=CC=CC=C2S

Technology Process of 2-[2-(2-Sulfanylphenyl)sulfanylethylsulfanyl]benzenethiol

There total 2 articles about 2-[2-(2-Sulfanylphenyl)sulfanylethylsulfanyl]benzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137-07-5
2-amino-benzenethiol

: 83209-89-6
1,2-bis(2-mercaptophenylthio)ethane

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Na / ethanol / 0.5 h / Heating

With sodium; In ethanol;

Reference yield:

: 87350-37-6
Fe(P(CH₃)3)2(SC₆H₄SC₂H₄SC₆H₄S)

: 106-93-4
ethylene dibromide

: 83209-89-6
1,2-bis(2-mercaptophenylthio)ethane

: 133616-67-8
2,3,8,9-dibenzo-1,4,7,10-tetrathiacyclododeka-2,8-diene

: 133616-68-9
2,3,8,9,14,15,20,21-tetrabenzo-1,4,7,10,13,16,19,22-octathiacyclotetracosa-2,8,14,20-tetraene

: 133616-69-0
2,3,8,9,14,15,20,21,26,27,32,33-hexabenzo-1,4,7,10,13,16,19,22,25,28,31,34-dodecathiacyclohexatriaconta-2,8,14,20,26,32-hexaene

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; N,N-dimethyl-formamide; to a soln. of Fe-compd. in DMF is added dropwise C2H4Br2 (50°C), the mixt. is stirred 22 h at 80°C, the suspn. is filtered and dried, addn. of boiling THF and HCl (reactions under N2); removing of volatile components in vac., the residue is extracted with CH2Cl2, removing of solvent, identification of products by spectroscopic methods (1H-NMR, FD-mass-spectra);