3-Bromo-5-[2-bromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-4-hydroxy-α-(hydroxyimino)benzenepropanamide

Base Information

Chemical Name:3-Bromo-5-[2-bromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-4-hydroxy-α-(hydroxyimino)benzenepropanamide
CAS No.:75513-48-3
Molecular Formula:C34H30Br4N4O8
Molecular Weight:942.24
Hs Code.:
Mol file:75513-48-3.mol

3-Bromo-5-[2-bromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-4-hydroxy-α-(hydroxyimino)benzenepropanamide

Synonyms:bastadin-1;3-[3-Bromo-5-(2-bromo-4-{2-[2-(3-bromo-4-hydroxy-phenyl)-ethylcarbamoyl]-2-[(E)-hydroxyimino]-ethyl}-phenoxy)-4-hydroxy-phenyl]-N-[2-(3-bromo-4-hydroxy-phenyl)-ethyl]-2-[(E)-hydroxyimino]-propionamide;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Bromo-5-[2-bromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-4-hydroxy-α-(hydroxyimino)benzenepropanamide

Chemical Property:

PSA：193.30000
LogP:7.89070

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 3-Bromo-5-[2-bromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-4-hydroxy-α-(hydroxyimino)benzenepropanamide

There total 9 articles about 3-Bromo-5-[2-bromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-4-hydroxy-α-(hydroxyimino)benzenepropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 83030-54-0
3-[3-Bromo-5-(2-bromo-4-{2-{2-[3-bromo-4-(4-methoxy-benzyloxy)-phenyl]-ethylcarbamoyl}-2-[(E)-hydroxyimino]-ethyl}-phenoxy)-4-hydroxy-phenyl]-N-{2-[3-bromo-4-(4-methoxy-benzyloxy)-phenyl]-ethyl}-2-[(E)-hydroxyimino]-propionamide

: 75513-48-3
prebastadin 1

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 0.333333h; Ambient temperature;
DOI:10.1016/S0040-4039(00)87083-5

Reference yield:

: 2973-78-6
3-bromo-4-hydroxybenzylaldehyde

: 75513-48-3
prebastadin 1

Guidance literature:: Multi-step reaction with 7 steps

2: K₂CO₃ / tetrahydrofuran / 18 h / Ambient temperature

3: 79 percent / Ac₂O, pyridine

4: 65 percent / NaBH₄ / bis-(2-methoxy-ethyl) ether / 1 h / 0 °C

5: Zn, AcOH / dioxane / 0.67 h / 0 - 5 °C

6: 34 percent / 41 h / 60 °C

7: 63 percent / trifluoroacetic acid / CH₂Cl₂ / 0.33 h / Ambient temperature

With pyridine; sodium tetrahydroborate; acetic anhydride; potassium carbonate; acetic acid; trifluoroacetic acid; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; diethylene glycol dimethyl ether;
DOI:10.1016/S0040-4039(00)87083-5

Reference yield:

: 937678-86-9
4-(4-methoxybenzyloxy)-3-bromobenzaldehyde

: 75513-48-3
prebastadin 1

Guidance literature:: Multi-step reaction with 6 steps

1: K₂CO₃ / tetrahydrofuran / 18 h / Ambient temperature

2: 79 percent / Ac₂O, pyridine

3: 65 percent / NaBH₄ / bis-(2-methoxy-ethyl) ether / 1 h / 0 °C

4: Zn, AcOH / dioxane / 0.67 h / 0 - 5 °C

5: 34 percent / 41 h / 60 °C

6: 63 percent / trifluoroacetic acid / CH₂Cl₂ / 0.33 h / Ambient temperature

With pyridine; sodium tetrahydroborate; acetic anhydride; potassium carbonate; acetic acid; trifluoroacetic acid; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; diethylene glycol dimethyl ether;
DOI:10.1016/S0040-4039(00)87083-5